Technology Process of C18H20N2O4S
There total 2 articles about C18H20N2O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at -40 - -20 ℃;
Inert atmosphere;
DOI:10.1039/c0ob00846j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 23 °C / Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran / -40 - -20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c0ob00846j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium acetate / ethanol; water / 24 h / Inert atmosphere; Darkness
2: trifluoroacetic acid / dichloromethane / Inert atmosphere
3: triethylamine / methanol / 6 h / 23 °C / Inert atmosphere
With
potassium acetate; triethylamine; trifluoroacetic acid;
In
methanol; ethanol; dichloromethane; water;
DOI:10.1039/c0ob00846j