C₁₇H₁₂NP

Base Information

Chemical Name:C₁₇H₁₂NP
CAS No.:1312012-29-5
Molecular Formula:C₁₇H₁₂NP
Molecular Weight:261.263
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₂NP

Chemical Property:

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Technology Process of C₁₇H₁₂NP

There total 6 articles about C₁₇H₁₂NP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312012-36-4
3-bromo-4-(2-bromophenyl)pyridine

: 644-97-3
Dichlorophenylphosphine

: 1312012-29-5
C₁₇H₁₂NP

Guidance literature:: 3-bromo-4-(2-bromophenyl)pyridine; With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 1h; Inert atmosphere;

Dichlorophenylphosphine; In diethyl ether; pentane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ic200951x

Reference yield:

: 4-(2-(diphenylphosphino)phenyl)pyridine

: 1312012-29-5
C₁₇H₁₂NP

Guidance literature:: With palladium diacetate; In toluene; at 160 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.201307115

Reference yield:

: 89167-19-1
3-bromo-4-iodopyridine

: 1312012-29-5
C₁₇H₁₂NP

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; potassium hydroxide / tetrahydrofuran; water / 72 h / Inert atmosphere; Reflux

2.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tert.-butyl lithium; potassium carbonate; potassium hydroxide; In tetrahydrofuran; diethyl ether; water; pentane; 1.1: Suzuki-Miyaura coupling;
DOI:10.1021/ic200951x