C₂₄H₄₂O₅Si

Base Information Edit

Chemical Name:C₂₄H₄₂O₅Si
CAS No.:1353389-29-3
Molecular Formula:C₂₄H₄₂O₅Si
Molecular Weight:438.68
Hs Code.:
Mol file:1353389-29-3.mol

C<sub>24</sub>H<sub>42</sub>O<sub>5</sub>Si

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Chemical Property of C₂₄H₄₂O₅Si Edit

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Technology Process of C₂₄H₄₂O₅Si

There total 7 articles about C₂₄H₄₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1343505-09-8
C₁₈H₃₀O₄

: 1353389-29-3
C₂₄H₄₂O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / -10 °C / Molecular sieve

2: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C

3: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

4: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

5: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

With 2,6-dimethylpyridine; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diisobutylaluminium hydride; Dess-Martin periodane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

: 1343505-20-3
C₂₄H₄₂O₄Si

: 1353389-29-3
C₂₄H₄₂O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

2: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

3: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diisobutylaluminium hydride; Dess-Martin periodane; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

: 1343505-16-7
C₁₈H₂₈O₄

: 1353389-29-3
C₂₄H₄₂O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C

2: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

3: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

4: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

With 2,6-dimethylpyridine; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diisobutylaluminium hydride; Dess-Martin periodane; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.158