C₃₃H₃₇NO₅Si

Base Information

Chemical Name:C₃₃H₃₇NO₅Si
CAS No.:1315471-33-0
Molecular Formula:C₃₃H₃₇NO₅Si
Molecular Weight:555.746
Hs Code.:

C<sub>33</sub>H<sub>37</sub>NO<sub>5</sub>Si

Synonyms:

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Chemical Property of C₃₃H₃₇NO₅Si

Chemical Property:

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Technology Process of C₃₃H₃₇NO₅Si

There total 12 articles about C₃₃H₃₇NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1315471-32-9
C₃₃H₃₆ClNO₅Si

: 1315471-33-0
C₃₃H₃₇NO₅Si

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 1.5h; diastereoselective reaction;
DOI:10.1021/jo201005d

Reference yield:

: 1025938-68-4
C₆H₈Br₂O₃

: 1315471-33-0
C₃₃H₃₇NO₅Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: toluene-4-sulfonic acid / 2 h / 18 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

2.2: 0.25 h

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 18 °C

3.2: 0.5 h / 0 - 18 °C

3.3: 0.5 h / 0 - 18 °C

4.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 2.5 h / Reflux

5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / tetrahydrofuran; water / 2 h / Reflux

6.1: acetic acid / water / 18 h / 50 °C

7.1: 1H-imidazole / N,N-dimethyl-formamide / 72 h

8.1: ammonia; hydrogen / methanol / 18 h / 18 °C

9.1: pyridine / dichloromethane / 0.25 h

10.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

10.2: 0.5 h / 18 °C

11.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimedone / tetrahydrofuran / 1 h / 18 °C

12.1: N-chloro-succinimide / dichloromethane / 1 h / -78 - 18 °C

13.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 1.5 h

With pyridine; 1H-imidazole; N-chloro-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 2,2'-azobis(isobutyronitrile); ammonia; hydrogen; tri-n-butyl-tin hydride; sodium hydride; dimedone; toluene-4-sulfonic acid; acetic acid; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene; 5.1: Suzuki-Miyaura cross-coupling;
DOI:10.1021/jo201005d

Reference yield:

: 1315471-04-5
C₁₁H₁₄BrNO₃

: 1315471-33-0
C₃₃H₃₇NO₅Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 18 °C

1.2: 0.5 h / 0 - 18 °C

1.3: 0.5 h / 0 - 18 °C

2.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 2.5 h / Reflux

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / tetrahydrofuran; water / 2 h / Reflux

4.1: acetic acid / water / 18 h / 50 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 72 h

6.1: ammonia; hydrogen / methanol / 18 h / 18 °C

7.1: pyridine / dichloromethane / 0.25 h

8.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

8.2: 0.5 h / 18 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimedone / tetrahydrofuran / 1 h / 18 °C

10.1: N-chloro-succinimide / dichloromethane / 1 h / -78 - 18 °C

11.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 1.5 h

With pyridine; 1H-imidazole; N-chloro-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 2,2'-azobis(isobutyronitrile); ammonia; hydrogen; tri-n-butyl-tin hydride; sodium hydride; dimedone; acetic acid; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene; 3.1: Suzuki-Miyaura cross-coupling;
DOI:10.1021/jo201005d