Technology Process of C30H50N4O4
There total 5 articles about C30H50N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrazine hydrate;
In
ethanol;
for 48h;
Reflux;
Inert atmosphere;
DOI:10.1039/c0jm01636e
- Guidance literature:
-
Multi-step reaction with 2 steps
1: nitric acid; acetic acid / dichloromethane / 0 - 20 °C
2: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 48 h / Reflux; Inert atmosphere
With
palladium 10% on activated carbon; nitric acid; hydrazine hydrate; acetic acid;
In
ethanol; dichloromethane;
DOI:10.1039/c0jm01636e
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / water
2: potassium carbonate / ethanol / 24 h / Inert atmosphere; Reflux
3: nitric acid; acetic acid / dichloromethane / 0 - 20 °C
4: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 48 h / Reflux; Inert atmosphere
With
palladium 10% on activated carbon; nitric acid; potassium carbonate; hydrazine hydrate; acetic acid; sodium hydroxide;
In
ethanol; dichloromethane; water;
DOI:10.1039/c0jm01636e