palladium(II) 5,10,15,20-tetraphenyl-21-benzocarbaporphyrin

Base Information

Chemical Name:palladium(II) 5,10,15,20-tetraphenyl-21-benzocarbaporphyrin
CAS No.:1323977-02-1
Molecular Formula:C₄₉H₃₁N₃Pd
Molecular Weight:768.225
Hs Code.:

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Chemical Property of palladium(II) 5,10,15,20-tetraphenyl-21-benzocarbaporphyrin

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Technology Process of palladium(II) 5,10,15,20-tetraphenyl-21-benzocarbaporphyrin

There total 4 articles about palladium(II) 5,10,15,20-tetraphenyl-21-benzocarbaporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: chloropalladium(II) 5,10,15,20-tetraphenyl-1,4-naphthiporphyrin

: 1323977-02-1
palladium(II) 5,10,15,20-tetraphenyl-21-benzocarbaporphyrin

: 1323976-99-3
palladium(II) 5,10,15,20-tetraphenyl-21-formyl-21-benzocarbaporphyrin

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1021/om2004139

Reference yield: 21.0%

: chloropalladium(II) 5,10,15,20-tetraphenyl-1,4-naphthiporphyrin

: 584-08-7
potassium carbonate

: 1323977-02-1
palladium(II) 5,10,15,20-tetraphenyl-21-benzocarbaporphyrin

: 1323976-99-3
palladium(II) 5,10,15,20-tetraphenyl-21-formyl-21-benzocarbaporphyrin

Guidance literature:: In acetonitrile; addn. of chloropalladium 5,10,15,20-tetraphenyl-1,4-naphthiporphyrin andK2CO3 to MeCN, stirring under N2 at room temp. overnight; evapn., chromy. (silica gel 70-230, dichloromethane), chromy. (silica gel 70-230, hexane/CH2Cl2 3/7 v/v);
DOI:10.1021/om2004139

Reference yield:

: 1312757-63-3
1,4-bis(phenylhydroxymethyl)naphthalene

: 1323977-02-1
palladium(II) 5,10,15,20-tetraphenyl-21-benzocarbaporphyrin

: 1323976-99-3
palladium(II) 5,10,15,20-tetraphenyl-21-formyl-21-benzocarbaporphyrin

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate / chloroform / Inert atmosphere; Reflux

2.1: boron trifluoride diethyl etherate / dichloromethane / 2 h / 20 °C / Inert atmosphere; Darkness

2.2: 0.5 h / Inert atmosphere; Darkness

3.1: palladium dichloride / acetonitrile / 48 h / 20 °C / Inert atmosphere

4.1: potassium carbonate / acetonitrile / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; potassium carbonate; palladium dichloride; In dichloromethane; chloroform; acetonitrile;
DOI:10.1021/om2004139