Technology Process of C27H26Cl3NO9
There total 6 articles about C27H26Cl3NO9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 12 h
2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane
With
1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
dichloromethane;
DOI:10.1016/j.tetlet.2011.04.060
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine; dmap / dichloromethane
2: hydrogenchloride; silica gel / water
3: triethylamine / dichloromethane / 12 h
4: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane
With
pyridine; hydrogenchloride; dmap; silica gel; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
dichloromethane; water;
DOI:10.1016/j.tetlet.2011.04.060
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Molecular sieve
2: sodium methylate / methanol; dichloromethane / 0 - 20 °C
3: pyridine; dmap / dichloromethane
4: hydrogenchloride; silica gel / water
5: triethylamine / dichloromethane / 12 h
6: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane
With
pyridine; hydrogenchloride; dmap; N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate; sodium methylate; silica gel; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
methanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2011.04.060
