C₆₈H₆₅Cl₂N₁₁O₁₀

Base Information

Chemical Name:C₆₈H₆₅Cl₂N₁₁O₁₀
CAS No.:633302-83-7
Molecular Formula:C₆₈H₆₅Cl₂N₁₁O₁₀
Molecular Weight:1267.24
Hs Code.:

C<sub>68</sub>H<sub>65</sub>Cl<sub>2</sub>N<sub>11</sub>O<sub>10</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₈H₆₅Cl₂N₁₁O₁₀

Chemical Property:

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Technology Process of C₆₈H₆₅Cl₂N₁₁O₁₀

There total 14 articles about C₆₈H₆₅Cl₂N₁₁O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67974-08-7
1-methyl-4-nitro-1H-pyrrole-2-carboxylic acid tert-butyl ester

: 633302-83-7
C₆₈H₆₅Cl₂N₁₁O₁₀

Guidance literature:: Multi-step reaction with 8 steps

1: H₂ / Pd/C / methanol / 2 h / 2585.81 Torr

2: 1.3 g / Et₃N / tetrahydrofuran / 2 h / 20 °C

3: H₂ / Pd/C / methanol / 2 h / 2585.81 Torr

4: 1.0 g / Et₃N / tetrahydrofuran / 2 h / 20 °C

5: H₂ / Pd/C / methanol / 2 h / 20 °C / 2585.81 Torr

6: 1.35 g / HOBt; EDCI / dimethylformamide / 12 h / 20 °C

7: 58 percent / TiCl₄ / CH₂Cl₂ / 24 h / 20 °C

8: 69 percent / HOBt; EDCI / dimethylformamide / 12 h / 20 °C

With hydrogen; titanium tetrachloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b303650m

Reference yield:

: 4-[(4-amino-1-methyl-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carboxylic acid tert-butyl ester

: 633302-83-7
C₆₈H₆₅Cl₂N₁₁O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: 1.0 g / Et₃N / tetrahydrofuran / 2 h / 20 °C

2: H₂ / Pd/C / methanol / 2 h / 20 °C / 2585.81 Torr

3: 1.35 g / HOBt; EDCI / dimethylformamide / 12 h / 20 °C

4: 58 percent / TiCl₄ / CH₂Cl₂ / 24 h / 20 °C

5: 69 percent / HOBt; EDCI / dimethylformamide / 12 h / 20 °C

With hydrogen; titanium tetrachloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b303650m

Reference yield:

: 13138-78-8
1-methyl-4-nitro-pyrrol-2-carboxylic acid

: 633302-83-7
C₆₈H₆₅Cl₂N₁₁O₁₀

Guidance literature:: Multi-step reaction with 9 steps

1: 82 percent / H₂SO₄ / diethyl ether / 36 h / 20 °C

2: H₂ / Pd/C / methanol / 2 h / 2585.81 Torr

3: 1.3 g / Et₃N / tetrahydrofuran / 2 h / 20 °C

4: H₂ / Pd/C / methanol / 2 h / 2585.81 Torr

5: 1.0 g / Et₃N / tetrahydrofuran / 2 h / 20 °C

6: H₂ / Pd/C / methanol / 2 h / 20 °C / 2585.81 Torr

7: 1.35 g / HOBt; EDCI / dimethylformamide / 12 h / 20 °C

8: 58 percent / TiCl₄ / CH₂Cl₂ / 24 h / 20 °C

9: 69 percent / HOBt; EDCI / dimethylformamide / 12 h / 20 °C

With sulfuric acid; hydrogen; titanium tetrachloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b303650m