C₃₁H₂₉N₂O₄S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₃₁H₂₉N₂O₄S^(1-)*Na⁽¹⁺⁾
CAS No.:1423693-19-9
Molecular Formula:C₃₁H₂₉N₂O₄S*Na
Molecular Weight:548.638
Hs Code.:

C<sub>31</sub>H<sub>29</sub>N<sub>2</sub>O<sub>4</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:

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Chemical Property of C₃₁H₂₉N₂O₄S^(1-)*Na⁽¹⁺⁾

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Technology Process of C₃₁H₂₉N₂O₄S^(1-)*Na⁽¹⁺⁾

There total 5 articles about C₃₁H₂₉N₂O₄S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1878-68-8
2-(4-bromophenyl)-acetic acid

: 1423693-19-9
C₃₁H₂₉N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / 16 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

2.2: 20 °C

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / Reflux; Inert atmosphere

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / Reflux; Inert atmosphere

5.1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C

5.2: pH 2

6.1: sodium hydroxide / methanol; acetonitrile / 0.33 h / 0 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; thionyl chloride; water; potassium acetate; sodium hydride; sodium carbonate; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; water; acetonitrile;

Reference yield:

: 1236357-64-4
methyl 1-(4-bromophenyl)cyclopentanecarboxylate

: 1423693-19-9
C₃₁H₂₉N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / Reflux; Inert atmosphere

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / Reflux; Inert atmosphere

3.1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C

3.2: pH 2

4.1: sodium hydroxide / methanol; acetonitrile / 0.33 h / 0 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; potassium acetate; sodium carbonate; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; water; acetonitrile;

Reference yield:

: 1423704-72-6
C₁₉H₂₇BO₄

: 1423693-19-9
C₃₁H₂₉N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 3 steps

1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / Reflux; Inert atmosphere

2.1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C

2.2: pH 2

3.1: sodium hydroxide / methanol; acetonitrile / 0.33 h / 0 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; sodium carbonate; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; acetonitrile;