C₂₈H₂₆

Base Information

Chemical Name:C₂₈H₂₆
CAS No.:135295-97-5
Molecular Formula:C₂₈H₂₆
Molecular Weight:362.514
Hs Code.:

Synonyms:

Suppliers and Price of C₂₈H₂₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₂₆

Chemical Property:

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Technology Process of C₂₈H₂₆

There total 4 articles about C₂₈H₂₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23697-29-2
9,10-Benzo-bicyclo[3.3.2]dec-9-en-3,7-dion

: 135295-97-5
C₂₈H₂₆

Guidance literature:: Multi-step reaction with 4 steps

1: 1) butyllithium / 1) THF, -70 deg C to 0 deg C, 2) THF, a) -70 deg C, 2 h, b) to room temp.

2: 100 percent / tetrahydrofuran / 24 h

3: 83 percent / Na/Hg, disodium hydrogen orthophosphate / tetrahydrofuran; methanol / 1) -70 deg C to -20 deg C, 2) -20 deg C, 3 h, 3) -20 deg C to room temp., 4) room temp, 8 h

4: toluene-p-sulphonic acid monohydrate / 52 h / 120 °C

With disodium hydrogenphosphate; sodium amalgam; n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;
DOI:10.1039/P19910001221

Reference yield:

: 135295-90-8
C₂₈H₂₈O₄S

: 135295-97-5
C₂₈H₂₆

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / tetrahydrofuran / 24 h

2: 83 percent / Na/Hg, disodium hydrogen orthophosphate / tetrahydrofuran; methanol / 1) -70 deg C to -20 deg C, 2) -20 deg C, 3 h, 3) -20 deg C to room temp., 4) room temp, 8 h

3: toluene-p-sulphonic acid monohydrate / 52 h / 120 °C

With disodium hydrogenphosphate; sodium amalgam; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;
DOI:10.1039/P19910001221

Reference yield:

: 135295-91-9
C₃₀H₂₇F₃O₅S

: 135295-97-5
C₂₈H₂₆

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Na/Hg, disodium hydrogen orthophosphate / tetrahydrofuran; methanol / 1) -70 deg C to -20 deg C, 2) -20 deg C, 3 h, 3) -20 deg C to room temp., 4) room temp, 8 h

2: toluene-p-sulphonic acid monohydrate / 52 h / 120 °C

With disodium hydrogenphosphate; sodium amalgam; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;
DOI:10.1039/P19910001221