Technology Process of C39H49N3O6
There total 10 articles about C39H49N3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere
2.1: diisobutylaluminium hydride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere
2.2: 0 °C / Inert atmosphere
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere
3.2: 6 h / -78 - 20 °C / Inert atmosphere
4.1: ethanol / 16 h / 20 °C / Inert atmosphere
5.1: sodium tetrahydroborate; ethanol / 5 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; oxalyl dichloride; ethanol; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane;
3.1: Swern oxidation / 3.2: Swern oxidation;
DOI:10.1021/ja2107564
- Guidance literature:
-
With
sodium tetrahydroborate; ethanol;
at 20 ℃;
for 5h;
Inert atmosphere;
DOI:10.1021/ja2107564
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisobutylaluminium hydride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere
1.2: 0 °C / Inert atmosphere
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere
2.2: 6 h / -78 - 20 °C / Inert atmosphere
3.1: ethanol / 16 h / 20 °C / Inert atmosphere
4.1: sodium tetrahydroborate; ethanol / 5 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; oxalyl dichloride; ethanol; diisobutylaluminium hydride; dimethyl sulfoxide;
In
tetrahydrofuran; ethanol; dichloromethane;
2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1021/ja2107564