IrCl(C₈H₁₂)(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

Base Information

• Chemical Name: IrCl(C₈H₁₂)(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)
• CAS No.: 145036-82-4
• Molecular Formula: C₄₄H₇₃ClIrP₃
• Molecular Weight: 922.658

Synonyms:

Chemical Property of IrCl(C₈H₁₂)(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of IrCl(C₈H₁₂)(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

There total 1 articles about IrCl(C₈H₁₂)(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

chloro(1,5-cyclooctadiene)iridium(I) dimer + Cyttp (70786-89-9) → IrCl(C8H12)(C6H5P(CH2CH2CH2P(C6H11)2)2) (145036-82-4)

Guidance literature:

In benzene; nitrogen atmosphere; benzene soln. of the ligand added to a benzene soln. of the Ir complex; stirring (0.5 h), removal of the solvent (vac.); solid suspended in hexane, collected on a frit, washed with hexane, dried in vac.; elem. anal.;

Reference yield: 40.0%

IrCl(C8H12)(C6H5P(CH2CH2CH2P(C6H11)2)2) (145036-82-4) → IrH2Cl(C6H5P(CH2CH2CH2P(C6H11)2)2) (103746-18-5)

Guidance literature:

With hydrogen; In benzene; nitrogen atmosphere; a soln. of the Ir complex (prepared in situ) is stirred for 0.5 h; hydrogen bubbled into the reaction mixt. (2 h); removal of the solvent in vac.; residue dissolved in THF; treatment with abs. ethanol; solid collected and dried in vac.; elem. anal.;

upstream raw materials:

Cyttp

Downstream raw materials:

IrH₂Cl(C₆H₅P(CH₂CH₂CH₂P(C₆H₁₁)2)2)

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