C₅H₅Fe(CO)2Si(CH₃)2Si(C₆H₅)3

Base Information

Chemical Name:C₅H₅Fe(CO)2Si(CH₃)2Si(C₆H₅)3
CAS No.:87882-62-0
Molecular Formula:C₂₇H₂₆FeO₂Si₂
Molecular Weight:494.52
Hs Code.:

C<sub>5</sub>H<sub>5</sub>Fe(CO)2Si(CH<sub>3</sub>)2Si(C<sub>6</sub>H<sub>5</sub>)3

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Chemical Property of C₅H₅Fe(CO)2Si(CH₃)2Si(C₆H₅)3

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Technology Process of C₅H₅Fe(CO)2Si(CH₃)2Si(C₆H₅)3

There total 1 articles about C₅H₅Fe(CO)2Si(CH₃)2Si(C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: sodium dicarbonyl(cyclopentadienyl)ferrate

: 69397-62-2
dimethyl(triphenylsilyl)chlorosilane

: 87882-62-0
C₅H₅Fe(CO)2Si(CH₃)2Si(C₆H₅)3

Guidance literature:: soln. of Fe-complex cooled to 0°C, added Si-compd., stirred for 90 min, warmed to room temp.; solvent removed (vac.), residue extracted (hexane/methylene), soln. concentrated, chromy. (SiO2), elem. anal.;
DOI:10.1021/ja00194a051

Reference yield: 85.0%

: 87882-62-0
C₅H₅Fe(CO)2Si(CH₃)2Si(C₆H₅)3

: FpSiMePh₂

: 41680-29-9
FpSiMe₂Ph

: 36835-55-9
(η⁵-C₅H₅)Fe(CO)₂SiPh₃

Guidance literature:: In cyclohexane; Irradiation (UV/VIS); photolyses for 1 h;; detected by HPLC;;
DOI:10.1021/ja00194a051

Reference yield:

: 87882-62-0
C₅H₅Fe(CO)2Si(CH₃)2Si(C₆H₅)3

: 101224-86-6
(C₆H₅)3SiSi(CH₃)2C₅H₄Fe(CO)2CH₃

Guidance literature:: With n-butyllithium; methyl iodide; In tetrahydrofuran; treatment of the complex in THF with a 2-fold excess of BuLi at -78°C, stirring for 2 h at the same temp., an excess of MeI is added, warming to room temp.; solvent removal, extn. (hexane), purified by column chromy. on alumina;