bis-([2-(4-((1-(2-(1-methoxy-1-oxo-3-phenylpropan-2-ylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methoxy)-benzyl)]-cyclopentadienyl) titanium(IV) dichloride

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Chemical Name:bis-([2-(4-((1-(2-(1-methoxy-1-oxo-3-phenylpropan-2-ylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methoxy)-benzyl)]-cyclopentadienyl) titanium(IV) dichloride
CAS No.:1331753-66-2
Molecular Formula:C₅₄H₅₄Cl₂N₈O₈Ti
Molecular Weight:1061.86
Hs Code.:

bis-([2-(4-((1-(2-(1-methoxy-1-oxo-3-phenylpropan-2-ylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methoxy)-benzyl)]-cyclopentadienyl) titanium(IV) dichloride

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Chemical Property of bis-([2-(4-((1-(2-(1-methoxy-1-oxo-3-phenylpropan-2-ylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methoxy)-benzyl)]-cyclopentadienyl) titanium(IV) dichloride

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Technology Process of bis-([2-(4-((1-(2-(1-methoxy-1-oxo-3-phenylpropan-2-ylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methoxy)-benzyl)]-cyclopentadienyl) titanium(IV) dichloride

There total 1 articles about bis-([2-(4-((1-(2-(1-methoxy-1-oxo-3-phenylpropan-2-ylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methoxy)-benzyl)]-cyclopentadienyl) titanium(IV) dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1173918-61-0
(rac)-methyl 2-(2-azidoacetamido)-3-phenylpropanoate

: 1331753-65-1
bis-[p-(prop-2-ynyloxy)-benzyl-cyclopentadienyl] titanium(IV) dichloride

: 1331753-66-2
bis-([2-(4-((1-(2-(1-methoxy-1-oxo-3-phenylpropan-2-ylamino)-2-oxoethyl)-1H-1,2,3-triazol-4-yl)methoxy)-benzyl)]-cyclopentadienyl) titanium(IV) dichloride

Guidance literature:: With catalyst: CuI/2,6-lutidine; In dichloromethane; acetonitrile; Ti-contg. compd. (0.16 mmol), N3-contg. compd. (0.34 mmol) and CuI (0.03mmol) were mixed and dissolved in CH2Cl2/CH3CN (2:1); after addn. of 2, 6-lutidine (0.34 mmol), the mixt. was degassed, purged with Ar and stirred for 12 h in the dark; the volatiles were removed; the solid was extd. with CHCl3; the vol. of the ext. was reduced and Et2O was added; the ppt. was sepd. by filtration and washed with Et2O and hexane and dried under reduced pressure; elem. anal.;
DOI:10.1016/j.poly.2011.05.036