(2S,3R,4R,5S)-(racemic)-5-(deuterophenylsulfonyl)-4-(6-(2-ethyl-t-butyldimethylsilylether)-3,4-methylenedioxyphenyl)-2,3-(isopropylidenedioxy)-5-(2-propenyl)cyclopentane

Base Information

Chemical Name:(2S,3R,4R,5S)-(racemic)-5-(deuterophenylsulfonyl)-4-(6-(2-ethyl-t-butyldimethylsilylether)-3,4-methylenedioxyphenyl)-2,3-(isopropylidenedioxy)-5-(2-propenyl)cyclopentane
CAS No.:112177-37-4
Molecular Formula:C₃₂H₄₄O₇SSi
Molecular Weight:601.841
Hs Code.:

(2S,3R,4R,5S)-(racemic)-5-(deuterophenylsulfonyl)-4-(6-(2-ethyl-t-butyldimethylsilylether)-3,4-methylenedioxyphenyl)-2,3-(isopropylidenedioxy)-5-(2-propenyl)cyclopentane

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Chemical Property of (2S,3R,4R,5S)-(racemic)-5-(deuterophenylsulfonyl)-4-(6-(2-ethyl-t-butyldimethylsilylether)-3,4-methylenedioxyphenyl)-2,3-(isopropylidenedioxy)-5-(2-propenyl)cyclopentane

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Technology Process of (2S,3R,4R,5S)-(racemic)-5-(deuterophenylsulfonyl)-4-(6-(2-ethyl-t-butyldimethylsilylether)-3,4-methylenedioxyphenyl)-2,3-(isopropylidenedioxy)-5-(2-propenyl)cyclopentane

There total 3 articles about (2S,3R,4R,5S)-(racemic)-5-(deuterophenylsulfonyl)-4-(6-(2-ethyl-t-butyldimethylsilylether)-3,4-methylenedioxyphenyl)-2,3-(isopropylidenedioxy)-5-(2-propenyl)cyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112177-35-2
{2-[6-((3aR,4R,5S,6aS)-5-Allyl-5-benzenesulfonyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxol-4-yl)-benzo[1,3]dioxol-5-yl]-ethoxy}-tert-butyl-dimethyl-silane

: 112177-37-4
(2S,3R,4R,5S)-(racemic)-5-(deuterophenylsulfonyl)-4-(6-(2-ethyl-t-butyldimethylsilylether)-3,4-methylenedioxyphenyl)-2,3-(isopropylidenedioxy)-5-(2-propenyl)cyclopentane

Guidance literature:: With water-d2; tert.-butyl lithium; In tetrahydrofuran; diethyl ether; at -78 ℃; for 1h;

Reference yield:

: C₁₅H₂₃LiO₃Si

: 112177-37-4
(2S,3R,4R,5S)-(racemic)-5-(deuterophenylsulfonyl)-4-(6-(2-ethyl-t-butyldimethylsilylether)-3,4-methylenedioxyphenyl)-2,3-(isopropylidenedioxy)-5-(2-propenyl)cyclopentane

Guidance literature:: Multi-step reaction with 2 steps

2: t-BuLi, D₂O / diethyl ether; tetrahydrofuran / 1 h / -78 °C

With water-d2; tert.-butyl lithium; In tetrahydrofuran; diethyl ether;

Reference yield:

: 105064-21-9
(2S,3R)-rac-2,3-(isopropylidenedioxy)-5-(phenylsulfonyl)-4-cyclopentene

: 112177-37-4
(2S,3R,4R,5S)-(racemic)-5-(deuterophenylsulfonyl)-4-(6-(2-ethyl-t-butyldimethylsilylether)-3,4-methylenedioxyphenyl)-2,3-(isopropylidenedioxy)-5-(2-propenyl)cyclopentane

Guidance literature:: Multi-step reaction with 2 steps

2: t-BuLi, D₂O / diethyl ether; tetrahydrofuran / 1 h / -78 °C

With water-d2; tert.-butyl lithium; In tetrahydrofuran; diethyl ether;