N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide

Base Information

Chemical Name:N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide
CAS No.:442543-02-4
Molecular Formula:C₂₇H₃₉NO₁₇
Molecular Weight:649.603
Hs Code.:

N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide

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Suppliers and Price of N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide

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Chemical Property of N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide

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Technology Process of N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide

There total 3 articles about N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121238-27-5
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl trichloroimidate

: 442543-02-4
N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 42 percent Chromat_. / TMSOTf / acetonitrile / -40 - 20 °C

2.1: H₂ / Pd(OH)2 / 0 °C

3.2: Zemplen's reagent

With trimethylsilyl trifluoromethanesulfonate; hydrogen; palladium dihydroxide; In acetonitrile; 1.1: Condensation / 2.1: Catalytic hydrogenation / 3.1: Acylation / 3.2: de-O-acetylation;
DOI:10.1080/07328300008544089

Reference yield:

: 273930-90-8
acetic acid 4,5-diacetoxy-6-acetoxymethyl-2-[3,5-dihydroxy-2-(4-nitro-phenoxy)-6-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3-yl ester

: 442543-02-4
N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / Pd(OH)2 / 0 °C

2.2: Zemplen's reagent

With hydrogen; palladium dihydroxide; 1.1: Catalytic hydrogenation / 2.1: Acylation / 2.2: de-O-acetylation;
DOI:10.1080/07328300008544089

Reference yield:

: acetic acid 4,5-diacetoxy-6-acetoxymethyl-2-[2-(4-amino-phenoxy)-3,5-dihydroxy-6-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3-yl ester

: 442543-02-4
N-{4-[(2R,3S,4S,5R,6R)-3,5-Dihydroxy-4-((2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-((2S,3S,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-phenyl}-acrylamide

Guidance literature:: acetic acid 4,5-diacetoxy-6-acetoxymethyl-2-[2-(4-amino-phenoxy)-3,5-dihydroxy-6-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3-yl ester; XCOCH=CH₂;

With Zemplen's reagent;
DOI:10.1080/07328300008544089