N-benzyl-N,N-dimethyl-N-<2-oxo-2-<5'-<13',21',29'-tris(bromoacetyl)-8',16',24',32'-tetramethyl<2.2.2.2>metacyclophano>>ethyl>ammonium bromide

Base Information

Chemical Name:N-benzyl-N,N-dimethyl-N-<2-oxo-2-<5'-<13',21',29'-tris(bromoacetyl)-8',16',24',32'-tetramethyl<2.2.2.2>metacyclophano>>ethyl>ammonium bromide
CAS No.:119878-08-9
Molecular Formula:Br*C₅₂H₅₅Br₃NO₄
Molecular Weight:1077.63
Hs Code.:

Synonyms:

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Chemical Property of N-benzyl-N,N-dimethyl-N-<2-oxo-2-<5'-<13',21',29'-tris(bromoacetyl)-8',16',24',32'-tetramethyl<2.2.2.2>metacyclophano>>ethyl>ammonium bromide

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Technology Process of N-benzyl-N,N-dimethyl-N-<2-oxo-2-<5'-<13',21',29'-tris(bromoacetyl)-8',16',24',32'-tetramethyl<2.2.2.2>metacyclophano>>ethyl>ammonium bromide

There total 6 articles about N-benzyl-N,N-dimethyl-N-<2-oxo-2-<5'-<13',21',29'-tris(bromoacetyl)-8',16',24',32'-tetramethyl<2.2.2.2>metacyclophano>>ethyl>ammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 119877-96-2
5,13,21,29-tetrakis(bromometyl)-8,16,24,32-tetramethyl<2.2.2.2>metacyclophane

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 119878-08-9
N-benzyl-N,N-dimethyl-N-<2-oxo-2-<5'-<13',21',29'-tris(bromoacetyl)-8',16',24',32'-tetramethyl<2.2.2.2>metacyclophano>>ethyl>ammonium bromide

Guidance literature:: In ethyl acetate; for 2h; Ambient temperature;
DOI:10.1021/jo00272a034

Reference yield:

: 67691-33-2
5,5'-di-tert-butyl-3,3'-bis(chloromethyl)-2,2'-dimethyldiphenylethane

: 119878-08-9
N-benzyl-N,N-dimethyl-N-<2-oxo-2-<5'-<13',21',29'-tris(bromoacetyl)-8',16',24',32'-tetramethyl<2.2.2.2>metacyclophano>>ethyl>ammonium bromide

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / CsOH, NaBH₄ / ethanol; benzene

2: 93 percent / m-chloroperbenzoic acid (MCPBA) / CH₂Cl₂ / 25 h / Ambient temperature

3: 93 percent / 500 °C / 0.4 - 0.5 Torr

4: 81 percent / AlCl₃, CH₃NO₂ / toluene / Ambient temperature

5: 26 percent / AlCl₃ / CS₂ / 4 h / Heating

6: 80 percent / ethyl acetate / 2 h / Ambient temperature

With cesium hydroxide; sodium tetrahydroborate; aluminium trichloride; nitromethane; 3-chloro-benzenecarboperoxoic acid; In carbon disulfide; ethanol; dichloromethane; ethyl acetate; toluene; benzene;
DOI:10.1021/jo00272a034

Reference yield:

: 119877-92-8
8,16,24,32-tetramethyl<2.2.2.2>metacyclophane

: 119878-08-9
N-benzyl-N,N-dimethyl-N-<2-oxo-2-<5'-<13',21',29'-tris(bromoacetyl)-8',16',24',32'-tetramethyl<2.2.2.2>metacyclophano>>ethyl>ammonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / AlCl₃ / CS₂ / 4 h / Heating

2: 80 percent / ethyl acetate / 2 h / Ambient temperature

With aluminium trichloride; In carbon disulfide; ethyl acetate;
DOI:10.1021/jo00272a034