2,4,6-tris(3-methylphenyl)-cyclo-1,3,5-trithia-2,4,6-triborinane

Base Information

Chemical Name:2,4,6-tris(3-methylphenyl)-cyclo-1,3,5-trithia-2,4,6-triborinane
CAS No.:156629-35-5
Molecular Formula:C₂₁H₂₁B₃S₃
Molecular Weight:402.029
Hs Code.:

Synonyms:

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Chemical Property of 2,4,6-tris(3-methylphenyl)-cyclo-1,3,5-trithia-2,4,6-triborinane

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Technology Process of 2,4,6-tris(3-methylphenyl)-cyclo-1,3,5-trithia-2,4,6-triborinane

There total 2 articles about 2,4,6-tris(3-methylphenyl)-cyclo-1,3,5-trithia-2,4,6-triborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 76782-89-3
3-CH₃C₆H₄BBr₂

: mercury sulfide

: 156629-35-5
2,4,6-tris(3-methylphenyl)-cyclo-1,3,5-trithia-2,4,6-triborinane

Guidance literature:: In benzene; byproducts: HgBr2; addn. of HgS to a soln. of B-compd. in dry benzene under N2, refluxing for 24 h; cooling to room temp., filtn. to remove HgBr2, evapn. to dryness;
DOI:10.1016/0022-328X(94)80027-8

Reference yield: 66.0%

: 76782-89-3
3-CH₃C₆H₄BBr₂

: 3385-94-2
hexamethyldisilathiane

: 156629-35-5
2,4,6-tris(3-methylphenyl)-cyclo-1,3,5-trithia-2,4,6-triborinane

Guidance literature:: In toluene; byproducts: Me3SiBr; N2-atmosphere; stirring at room temp. for 2 h; pptn. on cooling to -20°C overnight, decantation, drying (reducedpressure);
DOI:10.1016/0022-328X(94)05129-Y