C₅H₄CH(CH₃)2TiC₅H₃CH(CH₃)2B(C₆F₅)3

Base Information

• Chemical Name: C₅H₄CH(CH₃)2TiC₅H₃CH(CH₃)2B(C₆F₅)3
• CAS No.: 367251-64-7
• Molecular Formula: C₃₄H₂₁BF₁₅Ti
• Molecular Weight: 773.208

Synonyms:

Chemical Property of C₅H₄CH(CH₃)2TiC₅H₃CH(CH₃)2B(C₆F₅)3

Chemical Property:

Purity/Quality:

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Technology Process of C₅H₄CH(CH₃)2TiC₅H₃CH(CH₃)2B(C₆F₅)3

There total 1 articles about C₅H₄CH(CH₃)2TiC₅H₃CH(CH₃)2B(C₆F₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.1%

(iPrC5H4)2Ti(η2-Me3SiC2SiMe3) + tris(pentafluorophenyl)borate (1109-15-5) → C5H4CH(CH3)2TiC5H3CH(CH3)2B(C6F5)3 (367251-64-7)

Guidance literature:

In toluene; byproducts: bis(trimethylsilyl)acetylene, 1,2-bis(trimethylsilyl)ethane, 1,2-bis(trimethylsilyl)ethylene; (Ar); addn. of a soln. of boron compd. in toluene to a soln. of titaniumcomplex in toluene, stirring for 24 h; evapn. in vac., dissolving in hexane, filtration, keepin overnight at room temp., decantation, washing with hexane, drying at 20°C in vac.; elem. anal.;

DOI:10.1021/om0103052

Reference yield: 26.8%

C5H4CH(CH3)2TiC5H3CH(CH3)2B(C6F5)3 (367251-64-7) + oxygen (80937-33-3) + toluene (108-88-3,15644-74-3,16713-13-6) → [C5H4CH(CH3)2TiC5H3CH(CH3)2B(C6F5)3]2O*C6H5CH3

Guidance literature:

With air; In toluene; dissolving titanium complex in toluene at 60°C under Ar, cooling to room temp., filtration, exposing to dry air for 10-15 min, keeping at20°C overnight; decantation, washing with toluene, drying at 20°C in vac.; elem. anal.;

DOI:10.1021/om0103052

upstream raw materials:

tris(pentafluorophenyl)borate

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