2-carboxy-4,6-dimethoxydiphenylmethane

Base Information

Chemical Name:2-carboxy-4,6-dimethoxydiphenylmethane
CAS No.:90685-30-6
Molecular Formula:C₁₆H₁₆O₄
Molecular Weight:273.29
Hs Code.:

2-carboxy-4,6-dimethoxy<methylene-(13)C>diphenylmethane

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-carboxy-4,6-dimethoxydiphenylmethane

Chemical Property:

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Technology Process of 2-carboxy-4,6-dimethoxydiphenylmethane

There total 4 articles about 2-carboxy-4,6-dimethoxydiphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90685-29-3
2-carbomethoxy-4,6-dimethoxydiphenylmethane

: 90685-30-6
2-carboxy-4,6-dimethoxydiphenylmethane

Guidance literature:: With sodium hydroxide; In methanol; water; for 3h; Heating;
DOI:10.1016/S0031-9422(00)80323-4

Reference yield:

: 52947-05-4
[α-13C]benzoyl chloride

: 90685-30-6
2-carboxy-4,6-dimethoxydiphenylmethane

Guidance literature:: Multi-step reaction with 3 steps

1: 0.6 g / AlCl₃ / 24 h / Ambient temperature

2: 320 mg / Et₃SiH / trifluoroacetic acid / 48 h / Ambient temperature

3: 280 mg / 2M NaOH / methanol; H₂O / 3 h / Heating

With triethylsilane; sodium hydroxide; aluminium trichloride; In methanol; water; trifluoroacetic acid;
DOI:10.1016/S0031-9422(00)80323-4

Reference yield:

: 2150-37-0
methyl 3,5-dimethoxybenzoate

: 90685-30-6
2-carboxy-4,6-dimethoxydiphenylmethane

Guidance literature:: Multi-step reaction with 3 steps

1: 0.6 g / AlCl₃ / 24 h / Ambient temperature

2: 320 mg / Et₃SiH / trifluoroacetic acid / 48 h / Ambient temperature

3: 280 mg / 2M NaOH / methanol; H₂O / 3 h / Heating

With triethylsilane; sodium hydroxide; aluminium trichloride; In methanol; water; trifluoroacetic acid;
DOI:10.1016/S0031-9422(00)80323-4