[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]PF₆

Base Information

Chemical Name:[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]PF₆
CAS No.:691879-50-2
Molecular Formula:C₄₃H₇₅N₂OP₂Ru*F₆P
Molecular Weight:944.063
Hs Code.:

[Ru(CH=CH<sub>2</sub>)(CO)(NCCH<sub>3</sub>)2(P(Cy)3)2]PF<sub>6</sub>

Synonyms:

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Chemical Property of [Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]PF₆

Chemical Property:

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Technology Process of [Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]PF₆

There total 1 articles about [Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 17084-13-8
potassium hexafluorophosphate

: 691879-25-1
[RuCl(CH=CH₂)(CO)(P(Cy)3)2]

: 75-05-8,26809-02-9
acetonitrile

: 691879-50-2
[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]PF₆

Guidance literature:: In dichloromethane; under Ar; a soln. of Ru-contg. compd. (0.16 mmol) in CH2Cl2 was treated with KPF6 (0.54 mmol) and CH3CN (0.04 mol) and stirred for 20 min at room temp.; the solvent was evapd. in vac. and the residue was extd. twice with CH2Cl2; the combined exts. were dried in vac.; the solid was washed with pentane and dried; elem. anal.;
DOI:10.1039/b314425a

Reference yield: 67.0%

: 691879-50-2
[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]PF₆

: 143-66-8
sodium tetraphenyl borate

: 691879-56-8
[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]BPh₄

Guidance literature:: In methanol; under Ar; a suspn. of Ru-contg. compd. (0.12 mmol) in methanol was treated with NaBPh4 (0.73 mmol) and stirred for 1 h at room temp.; the solvent was evapd. in vac. and the residue was washed twice with methanol and then dissolved in CH2Cl2; the soln. was filtered and the filtrate was brought to dryness in vac.; the solid was washed twice with pentane and dried; elem. anal.;
DOI:10.1039/b314425a