[Pd(tosylmethyl isocyanide)2(C(Me)N(CH₂tosyl))Cl]

Base Information

Chemical Name:[Pd(tosylmethyl isocyanide)2(C(Me)N(CH₂tosyl))Cl]
CAS No.:958877-56-0
Molecular Formula:C₂₈H₃₀ClN₃O₆PdS₃
Molecular Weight:742.634
Hs Code.:

[Pd(tosylmethyl isocyanide)2(C(Me)N(CH<sub>2</sub>tosyl))Cl]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Pd(tosylmethyl isocyanide)2(C(Me)N(CH₂tosyl))Cl]

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Technology Process of [Pd(tosylmethyl isocyanide)2(C(Me)N(CH₂tosyl))Cl]

There total 3 articles about [Pd(tosylmethyl isocyanide)2(C(Me)N(CH₂tosyl))Cl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 38622-91-2,36635-61-7
[(p-methylphenyl)sulfonylmethyl]isonitrile

: 958877-56-0
[Pd(tosylmethyl isocyanide)2(C(Me)N(CH₂tosyl))Cl]

Guidance literature:: In dichloromethane; byproducts: C8H12; addn. of tosylmethyl isocyanide (3 equiv.) to Pd(COD)Me(Cl) in CH2Cl2 under Ar; stirring for 1 h; drying under vac., treatment with Et2O; washing twice with small aliquots of Et2O; and with pentane; elem. anal.;
DOI:10.1021/om700555a

Reference yield:

: 460720-26-7
[Pd(2-methylthiomethylpyridine)(methyl)Cl]

: 38622-91-2,36635-61-7
[(p-methylphenyl)sulfonylmethyl]isonitrile

: 958877-56-0
[Pd(tosylmethyl isocyanide)2(C(Me)N(CH₂tosyl))Cl]

Guidance literature:: In chloroform-d1; byproducts: 2-methylthiomethylpyridine; treatment of PdCl(Me)(C5H4NCH2SMe) with tosylmethyl isocyanide (3 equiv.) in CDCl3 at 298 K;
DOI:10.1021/om700555a