Acetic acid (2R,3R,4R,5R,6R)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

Base Information

Chemical Name:Acetic acid (2R,3R,4R,5R,6R)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester
CAS No.:189108-65-4
Molecular Formula:C₃₈H₅₂N₄O₁₈
Molecular Weight:852.847
Hs Code.:

Acetic acid (2R,3R,4R,5R,6R)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

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Chemical Property of Acetic acid (2R,3R,4R,5R,6R)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

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Technology Process of Acetic acid (2R,3R,4R,5R,6R)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

There total 4 articles about Acetic acid (2R,3R,4R,5R,6R)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (2R,3R,4R,5R)-2-acetoxymethyl-5-azido-6-nitro-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

: 189108-65-4
Acetic acid (2R,3R,4R,5R,6R)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiBr / acetonitrile / 3 h

2: ZnBr₂

With lithium bromide; zinc dibromide; In acetonitrile;
DOI:10.1016/S0008-6215(96)00309-6

Reference yield:

: 189108-63-2
4,6-di-O-acetyl-2-azido-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyl iodide

: 189108-65-4
Acetic acid (2R,3R,4R,5R,6R)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / (C₂H₅)4NCl

2: AgOTf / CH₂Cl₂

With tetraethylammonium chloride; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1016/S0008-6215(96)00309-6

Reference yield:

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 166108-25-4
2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1[*]3)-4,6-di-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl chloride

: 189108-65-4
Acetic acid (2R,3R,4R,5R,6R)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

: Acetic acid (2R,3R,4R,5R,6S)-2-acetoxymethyl-5-azido-6-(6-benzyloxycarbonylamino-hexyloxy)-4-((2R,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; Yield given. Yields of byproduct given;
DOI:10.1016/S0008-6215(96)00309-6