C₂₉H₄₀O₇S

Base Information

Chemical Name:C₂₉H₄₀O₇S
CAS No.:1373885-45-0
Molecular Formula:C₂₉H₄₀O₇S
Molecular Weight:532.698
Hs Code.:

C<sub>29</sub>H<sub>40</sub>O<sub>7</sub>S

Synonyms:

Suppliers and Price of C₂₉H₄₀O₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₄₀O₇S

Chemical Property:

Purity/Quality:

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Technology Process of C₂₉H₄₀O₇S

There total 16 articles about C₂₉H₄₀O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₄O₅

: 98-59-9
p-toluenesulfonyl chloride

: 1373885-45-0
C₂₉H₄₀O₇S

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 168h;
DOI:10.1016/j.tetlet.2012.02.090

Reference yield:

: 1373885-32-5
C₁₈H₂₆O₅

: 1373885-45-0
C₂₉H₄₀O₇S

Guidance literature:: Multi-step reaction with 15 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

2: 1H-imidazole; iodine; triphenylphosphine / toluene / 20 h / 20 °C

3: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 4 h / -40 - 20 °C

4: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 72 h / 20 °C

5: sodium periodate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C

6: zinc trifluoromethanesulfonate; triethylamine / toluene / 48 h / 20 - 60 °C

7: methanol; potassium carbonate / 15 h / 20 °C

8: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

9: 1H-imidazole / dichloromethane / 5 h / 0 - 20 °C

10: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 120 h / 20 °C

11: N-iodo-succinimide; triphenylphosphine / tetrahydrofuran / 3 h / 0 - 20 °C

12: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 7 h / -40 - 20 °C

13: toluene-4-sulfonic acid / dichloromethane / 8 h / 0 - 20 °C

14: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 0 - 20 °C

15: dmap; triethylamine / dichloromethane / 168 h / 0 - 20 °C

With 1H-imidazole; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; sodium periodate; N-iodo-succinimide; copper(l) iodide; osmium(VIII) oxide; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; water; iodine; zinc trifluoromethanesulfonate; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; 6: Carreira's addition;
DOI:10.1016/j.tetlet.2012.02.090

Reference yield:

: C₁₈H₂₈O₅

: 1373885-45-0
C₂₉H₄₀O₇S

Guidance literature:: Multi-step reaction with 11 steps

1: sodium periodate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C

2: zinc trifluoromethanesulfonate; triethylamine / toluene / 48 h / 20 - 60 °C

3: methanol; potassium carbonate / 15 h / 20 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

5: 1H-imidazole / dichloromethane / 5 h / 0 - 20 °C

6: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 120 h / 20 °C

7: N-iodo-succinimide; triphenylphosphine / tetrahydrofuran / 3 h / 0 - 20 °C

8: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 7 h / -40 - 20 °C

9: toluene-4-sulfonic acid / dichloromethane / 8 h / 0 - 20 °C

10: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 0 - 20 °C

11: dmap; triethylamine / dichloromethane / 168 h / 0 - 20 °C

With 1H-imidazole; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; sodium periodate; N-iodo-succinimide; copper(l) iodide; osmium(VIII) oxide; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; water; zinc trifluoromethanesulfonate; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; 2: Carreira's addition;
DOI:10.1016/j.tetlet.2012.02.090