C₂₇H₃₄N₂O₆

Base Information

• Chemical Name: C₂₇H₃₄N₂O₆
• CAS No.: 1383737-77-6
• Molecular Formula: C₂₇H₃₄N₂O₆
• Molecular Weight: 482.577
• Mol file: 1383737-77-6.mol

Synonyms:

Chemical Property of C₂₇H₃₄N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₃₄N₂O₆

There total 1 articles about C₂₇H₃₄N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H23NO4 (1383737-76-5) + 1-nitropentane (628-05-7) → C27H34N2O6 (1383737-77-6)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1016/j.bmcl.2012.04.106

Reference yield:

C27H34N2O6 (1383737-77-6) → C27H32N2O5 (1383737-79-8)

Guidance literature:

C₂₇H₃₄N₂O₆; With dmap; acetic anhydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

In dichloromethane; at 20 ℃; for 16h;

DOI:10.1016/j.bmcl.2012.04.106

Reference yield:

C27H34N2O6 (1383737-77-6) → C43H45N3O6 (1383737-85-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: dmap; acetic anhydride / tetrahydrofuran / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / -78 °C

2.2: 2 h / -78 °C

With dmap; potassium tert-butylate; acetic anhydride; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2012.04.106

upstream raw materials:

C₂₂H₂₃NO₄

1-nitropentane

Downstream raw materials:

C₂₇H₃₂N₂O₅

C₄₃H₄₅N₃O₆

C₄₃H₄₅N₃O₆

C₄₄H₄₂N₄O₇S