N,N'-bis(mesityl)-2,3;6,7-(OOBPh)2-1,4,5,8-naphthalenediimide

Base Information

Chemical Name:N,N'-bis(mesityl)-2,3;6,7-(OOBPh)2-1,4,5,8-naphthalenediimide
CAS No.:1352239-26-9
Molecular Formula:C₄₄H₃₂B₂N₂O₈
Molecular Weight:738.369
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(mesityl)-2,3;6,7-(OOBPh)2-1,4,5,8-naphthalenediimide

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Technology Process of N,N'-bis(mesityl)-2,3;6,7-(OOBPh)2-1,4,5,8-naphthalenediimide

There total 3 articles about N,N'-bis(mesityl)-2,3;6,7-(OOBPh)2-1,4,5,8-naphthalenediimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1259935-85-7
N,N-dimesityl-2,3,6,7-tetrabromo-naphthalene-1,4,5,8-tetracarboxylic acid bisimide

: 1352239-26-9
N,N'-bis(mesityl)-2,3;6,7-(OOBPh)2-1,4,5,8-naphthalenediimide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / dichloromethane / 12 h / 20 °C / Inert atmosphere; Molecular sieve

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane / dichloromethane / 16 h / 20 °C / Inert atmosphere; Molecular sieve

3: water; dimethyl sulfoxide / 0.03 h / 20 °C / pH 8 / Inert atmosphere; aq. buffer

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; sodium hydride; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1039/c1ob05702b

Reference yield:

: 1352239-15-6
N,N'-bis(mesityl)-2,3,6,7-tetrahydroxy-1,4,5,8-naphthalenediimide

: 98-80-6
phenylboronic acid

: 1352239-26-9
N,N'-bis(mesityl)-2,3;6,7-(OOBPh)2-1,4,5,8-naphthalenediimide

Guidance literature:: In water; dimethyl sulfoxide; at 20 ℃; for 0.0333333h; pH=8; Inert atmosphere; aq. buffer;
DOI:10.1039/c1ob05702b

Reference yield:

: N,N'-bis(mesityl)-2,3-(O₂B(OH)Ph)-6,7-(O₂BPh)-1,4,5,8-naphthalenediimide^(1-)

: 1352239-26-9
N,N'-bis(mesityl)-2,3;6,7-(OOBPh)2-1,4,5,8-naphthalenediimide

Guidance literature:: With H⁽¹⁺⁾; In water; dimethyl sulfoxide; addn. of acid to soln. of B compd. in DMSO/water (4/1); detected by UV spectroscopy;
DOI:10.1039/c1ob05702b