methyl 4-hydroxymethyl-2,3,5,6-tetradeuterobenzoate

Base Information

Chemical Name:methyl 4-hydroxymethyl-2,3,5,6-tetradeuterobenzoate
CAS No.:1365183-52-3
Molecular Formula:C₉H₁₀O₃
Molecular Weight:170.145
Hs Code.:

Synonyms:

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Chemical Property of methyl 4-hydroxymethyl-2,3,5,6-tetradeuterobenzoate

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Technology Process of methyl 4-hydroxymethyl-2,3,5,6-tetradeuterobenzoate

There total 3 articles about methyl 4-hydroxymethyl-2,3,5,6-tetradeuterobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₆⁽²⁾H₄N₂O₃

: 1365183-52-3
methyl 4-hydroxymethyl-2,3,5,6-tetradeuterobenzoate

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 ℃; for 0.5h;
DOI:10.1039/c2cc00027j

Reference yield:

: 74079-01-9
2,3,5,6-tetradeuterio-terephthalic acid dimethyl ester

: 1365183-52-3
methyl 4-hydroxymethyl-2,3,5,6-tetradeuterobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; potassium hydroxide / 4 h / Reflux

2: tetrahydrofuran / 0.17 h / 20 °C

3: sodium tetrahydroborate / tetrahydrofuran; water / 0.5 h / 0 °C

With methanol; sodium tetrahydroborate; potassium hydroxide; In tetrahydrofuran; water;
DOI:10.1039/c2cc00027j

Reference yield:

: 60088-54-2
2,3,5,6-tetradeuteroterephthalic acid

: 1365183-52-3
methyl 4-hydroxymethyl-2,3,5,6-tetradeuterobenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 3 h / Reflux

2: methanol; potassium hydroxide / 4 h / Reflux

3: tetrahydrofuran / 0.17 h / 20 °C

4: sodium tetrahydroborate / tetrahydrofuran; water / 0.5 h / 0 °C

With methanol; sodium tetrahydroborate; thionyl chloride; potassium hydroxide; In tetrahydrofuran; water;
DOI:10.1039/c2cc00027j