methyl 2-deoxy-3,5-di-O-p-toluoyl-D-erythro-pentose-2,2',3,4-²H₄

Base Information

Chemical Name:methyl 2-deoxy-3,5-di-O-p-toluoyl-D-erythro-pentose-2,2',3,4-²H₄
CAS No.:116217-37-9
Molecular Formula:C₂₂H₂₄O₆
Molecular Weight:388.397
Hs Code.:

methyl 2-deoxy-3,5-di-O-p-toluoyl-D-erythro-pentose-2,2',3,4-<sup>2</sup>H<sub>4</sub>

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Chemical Property of methyl 2-deoxy-3,5-di-O-p-toluoyl-D-erythro-pentose-2,2',3,4-²H₄

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Technology Process of methyl 2-deoxy-3,5-di-O-p-toluoyl-D-erythro-pentose-2,2',3,4-²H₄

There total 9 articles about methyl 2-deoxy-3,5-di-O-p-toluoyl-D-erythro-pentose-2,2',3,4-²H₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5328-63-2
methyl-β-D-arabinopyranoside

: 116217-37-9,116217-54-0
methyl 2-deoxy-3,5-di-O-p-toluoyl-D-erythro-pentose-2,2',3,4-²H₄

Guidance literature:: Multi-step reaction with 8 steps

1: 33 percent / deuterium oxide / deuterated Raney nickel / 15 h / Heating

2: 90 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 3 h / 20 °C

3: 86 percent / N,N-dimethylaminopyridine / acetonitrile / 20 °C

4: tri-n-butyltin-deuteride, 2,2'-azo-bis-(2-methylpropionitrile) / toluene / 2 h / 80 °C

5: 80percent acetic acid / 15 h / 20 °C

6: 0.5 M HCl / 40 h / 20 °C

7: HCl

8: pyridine

With pyridine; hydrogenchloride; dmap; 2,2'-azobis(isobutyronitrile); water-d2; tributyltin deuteride; toluene-4-sulfonic acid; acetic acid; deuterated Raney nickel; In N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/S0040-4020(01)83465-7

Reference yield:

: 116217-31-3
3,4-isopropylidene methyl-β-D-arabinopyranoside-2,3,4-²H₃

: 116217-37-9,116217-54-0
methyl 2-deoxy-3,5-di-O-p-toluoyl-D-erythro-pentose-2,2',3,4-²H₄

Guidance literature:: Multi-step reaction with 6 steps

1: 86 percent / N,N-dimethylaminopyridine / acetonitrile / 20 °C

2: tri-n-butyltin-deuteride, 2,2'-azo-bis-(2-methylpropionitrile) / toluene / 2 h / 80 °C

3: 80percent acetic acid / 15 h / 20 °C

4: 0.5 M HCl / 40 h / 20 °C

5: HCl

6: pyridine

With pyridine; hydrogenchloride; dmap; 2,2'-azobis(isobutyronitrile); tributyltin deuteride; acetic acid; In toluene; acetonitrile;
DOI:10.1016/S0040-4020(01)83465-7

Reference yield:

: 116217-30-2
methyl-β-D-arabinopyranoside-2,3,4-²H₃

: 116217-37-9,116217-54-0
methyl 2-deoxy-3,5-di-O-p-toluoyl-D-erythro-pentose-2,2',3,4-²H₄

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 3 h / 20 °C

2: 86 percent / N,N-dimethylaminopyridine / acetonitrile / 20 °C

3: tri-n-butyltin-deuteride, 2,2'-azo-bis-(2-methylpropionitrile) / toluene / 2 h / 80 °C

4: 80percent acetic acid / 15 h / 20 °C

5: 0.5 M HCl / 40 h / 20 °C

6: HCl

7: pyridine

With pyridine; hydrogenchloride; dmap; 2,2'-azobis(isobutyronitrile); tributyltin deuteride; toluene-4-sulfonic acid; acetic acid; In N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/S0040-4020(01)83465-7