Technology Process of C25H36N2
There total 3 articles about C25H36N2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: methanol / 4 h / 20 °C
2.1: sodium tetrahydroborate / methanol / 3 h / 20 °C
3.1: phosphoric acid / water; dichloromethane / 4 h / 20 °C
4.1: methanol / 20 °C / Inert atmosphere
4.2: 20 °C
With
sodium tetrahydroborate; phosphoric acid;
In
methanol; dichloromethane; water;
DOI:10.1002/ardp.201200219
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: phosphoric acid / water; dichloromethane / 4 h / 20 °C
2.1: methanol / 20 °C / Inert atmosphere
2.2: 20 °C
With
phosphoric acid;
In
methanol; dichloromethane; water;
DOI:10.1002/ardp.201200219
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1,4-dioxane / 22 h / 20 °C
2.1: methanol / 4 h / 20 °C
3.1: sodium tetrahydroborate / methanol / 3 h / 20 °C
4.1: phosphoric acid / water; dichloromethane / 4 h / 20 °C
5.1: methanol / 20 °C / Inert atmosphere
5.2: 20 °C
With
sodium tetrahydroborate; phosphoric acid;
In
1,4-dioxane; methanol; dichloromethane; water;
DOI:10.1002/ardp.201200219