TlOCPh₃

Base Information

Chemical Name:TlOCPh₃
CAS No.:853178-75-3
Molecular Formula:C₁₉H₁₅O*Tl
Molecular Weight:463.711
Hs Code.:

Synonyms:

Suppliers and Price of TlOCPh₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of TlOCPh₃

Chemical Property:

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Technology Process of TlOCPh₃

There total 1 articles about TlOCPh₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 20398-06-5
thallium (I) ethoxide

: 853178-75-3
TlOCPh₃

Guidance literature:: In petroleum ether; Schlenk or glovebox techniquie, under N2; HOCPh3 (0.2 g) dissolved in petroleum ether (10 ml) and minimal amt. of THF (if necessary); soln. of thallium ethoxide (one equiv.) in petroleum ether (4 ml) added; stirred in dark; ppt. collected; washed with petroleum ether; dried;
DOI:10.1021/ja045310m

Reference yield: 18.0%

: 388110-50-7
[PhBP₃]CoI

: 853178-75-3
TlOCPh₃

: [PhBP₃]CoOCPh₃

Guidance literature:: In tetrahydrofuran; byproducts: TlI; Schlenk or glavebox technique, under N2; THF (3 ml) soln. of TlOCPh3 (0.267 mmol) added to stirring soln. of Co complex (0.267 mmol) in THF (10 ml); stirred (4 h); TlI filtered off; THF removed (vac.); washed with petroleum ether; dried; dissolved in benzene (4 ml); triturated with petroleum ether (15 ml); supernatant sepd.; dried (vac.); crystd. by vapor diffusion of petroleumether in benzene soln.; elem. anal.;
DOI:10.1021/ja045310m