1β,2β,3α,5αβ-tetraacetoxycyclohexane

Base Information

Chemical Name:1β,2β,3α,5αβ-tetraacetoxycyclohexane
CAS No.:66325-66-4
Molecular Formula:C₁₄H₂₀O₈
Molecular Weight:316.308
Hs Code.:

Synonyms:

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Chemical Property of 1β,2β,3α,5αβ-tetraacetoxycyclohexane

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Technology Process of 1β,2β,3α,5αβ-tetraacetoxycyclohexane

There total 5 articles about 1β,2β,3α,5αβ-tetraacetoxycyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 89025-64-9,102720-50-3
1αβ,3β,4β,5α-tetraacetoxy-1αβ(2'-pyridylthio)cyclohexane

: 66325-66-4,89025-63-8,92298-56-1
1β,2β,3α,5αβ-tetraacetoxycyclohexane

Guidance literature:: With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile); In toluene; at 110 ℃; for 1h; adding 15 min;
DOI:10.1016/S0040-4020(01)97173-X

Reference yield:

: 23804-28-6,32469-24-2,62445-00-5
(-)-1,3,4,5-Tetra-O-acetylquinic acid

: 66325-66-4,89025-63-8,92298-56-1
1β,2β,3α,5αβ-tetraacetoxycyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: oxalylchloride / DMF / benzene / 2 h / Ambient temperature

2: DMAP / toluene / 2 h / 110 °C

3: 57 percent / tri-n-butylstannane / AIBN / toluene / 1 h / 110 °C / adding 15 min

With Chloro-oxo-acetic acid; tri-n-butyl-tin hydride; dmap; 2,2'-azobis(isobutyronitrile); N,N-dimethyl-formamide; In toluene; benzene;
DOI:10.1016/S0040-4020(01)97173-X

Reference yield:

: 92651-21-3,92822-51-0,95463-24-4
Acetic acid (3R,5R)-3,4,5-triacetoxy-1-chlorocarbonyl-cyclohexyl ester

: 66325-66-4,89025-63-8,92298-56-1
1β,2β,3α,5αβ-tetraacetoxycyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / toluene / 2 h / 110 °C

2: 57 percent / tri-n-butylstannane / AIBN / toluene / 1 h / 110 °C / adding 15 min

With tri-n-butyl-tin hydride; dmap; 2,2'-azobis(isobutyronitrile); In toluene;
DOI:10.1016/S0040-4020(01)97173-X