Benzene, 1-[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxy-

Base Information

Chemical Name:Benzene, 1-[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxy-
CAS No.:120233-90-1
Molecular Formula:C21H28O5
Molecular Weight:360.45
Hs Code.:
DSSTox Substance ID:DTXSID80450261
Nikkaji Number:J2.010.154G
Wikidata:Q82269888
Mol file:120233-90-1.mol

Synonyms:120233-90-1;Benzene, 1-[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxy-;SCHEMBL9301138;DTXSID80450261;1-[4-(3,4-Dimethoxyphenyl)butyl]-2,3,4-trimethoxybenzene

Suppliers and Price of Benzene, 1-[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxy-

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:10
Exact Mass:360.19367399
Heavy Atom Count:26
Complexity:377

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)CCCCC2=C(C(=C(C=C2)OC)OC)OC)OC

Technology Process of Benzene, 1-[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxy-

There total 3 articles about Benzene, 1-[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-[(Z)-4-(3,4-Dimethoxy-phenyl)-but-1-enyl]-2,3,4-trimethoxy-benzene

: 120233-90-1
[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxybenzene

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/ejoc.200300263

Reference yield:

: 118156-83-5
3-(3,4-dimethoxyphenyl)-1-iodopropane

: 120233-90-1
[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 84 percent / dimethylformamide / 4 h / Heating

2.1: potassium tert-butoxide / tetrahydrofuran / 2 h / 0 °C

2.2: tetrahydrofuran

3.1: 3.76 g / H₂ / Pd/C / tetrahydrofuran / 12 h / 20 °C

With potassium tert-butylate; hydrogen; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200300263

Reference yield:

: [3-(3,4-dimethoxyphenyl)propyl]triphenylphosphonium iodide

: 120233-90-1
[4-(3,4-dimethoxyphenyl)butyl]-2,3,4-trimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butoxide / tetrahydrofuran / 2 h / 0 °C

1.2: tetrahydrofuran

2.1: 3.76 g / H₂ / Pd/C / tetrahydrofuran / 12 h / 20 °C

With potassium tert-butylate; hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1002/ejoc.200300263