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Technology Process of (C6H4-4-CH3O)2BN3

(C6H4-4-CH3O)2BN3

Base Information
  • Chemical Name:(C6H4-4-CH3O)2BN3
  • CAS No.:13272-65-6
  • Molecular Formula:C14H14BN3O2
  • Molecular Weight:267.095
  • Hs Code.:
(C<sub>6</sub>H<sub>4</sub>-4-CH<sub>3</sub>O)2BN<sub>3</sub>

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Chemical Property of (C6H4-4-CH3O)2BN3
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Technology Process of (C6H4-4-CH3O)2BN3

There total 3 articles about (C6H4-4-CH3O)2BN3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ClB(C<sub>6</sub>H<sub>4</sub>-4-OCH<sub>3</sub>)2
13272-76-9

ClB(C6H4-4-OCH3)2

(C<sub>6</sub>H<sub>4</sub>-4-CH<sub>3</sub>O)2BN<sub>3</sub>
13272-65-6

(C6H4-4-CH3O)2BN3

Guidance literature:
With lithium azide; In benzene;
DOI:10.1016/S0022-328X(00)90824-6

Reference yield:

C<sub>28</sub>H<sub>28</sub>B<sub>2</sub>O<sub>5</sub>

C28H28B2O5

(C<sub>6</sub>H<sub>4</sub>-4-CH<sub>3</sub>O)2BN<sub>3</sub>
13272-65-6

(C6H4-4-CH3O)2BN3

Guidance literature:
Multi-step reaction with 2 steps
1: BCl3 / CH2Cl2 / -80 °C
2: LiN3 / benzene
With lithium azide; boron trichloride; In dichloromethane; benzene;
DOI:10.1016/S0022-328X(00)90824-6

Reference yield:

(C<sub>6</sub>H<sub>4</sub>-4-CH<sub>3</sub>O)2BN<sub>3</sub>
13272-65-6

(C6H4-4-CH3O)2BN3

Guidance literature:
Pyridinat C14H14BN3O2*C5H5N, Δ im geschloss. Rohr auf 200grad/2 h unter N2-Abspaltung, (neben Harzprodd. u. Hexa-<4-methoxy-phenyl>-borazol);
DOI:10.1016/S0022-328X(00)90825-8
upstream raw materials:

ClB(C6H4-4-OCH3)2

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