Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-6-O-(4,6-di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-β-D-glucopyranosid

Base Information

Chemical Name:Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-6-O-(4,6-di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-β-D-glucopyranosid
CAS No.:106115-83-7
Molecular Formula:C₄₄H₄₈N₆O₁₁
Molecular Weight:842.851
Hs Code.:

Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-6-O-(4,6-di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-β-D-glucopyranosid

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Chemical Property of Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-6-O-(4,6-di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-β-D-glucopyranosid

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Technology Process of Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-6-O-(4,6-di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-β-D-glucopyranosid

There total 5 articles about Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-6-O-(4,6-di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-β-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106115-79-1
4,6-Di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

: 106115-82-6
Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid

: 106115-83-7
Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-6-O-(4,6-di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-β-D-glucopyranosid

Guidance literature:: With silver silicate; 4 A molecular sieve; In dichloromethane; at -20 ℃; for 2.5h;

Reference yield:

: 106139-07-5
6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

: 106115-83-7
Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-6-O-(4,6-di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / silver silicate, molecular sieve 4 Angstroem / CH₂Cl₂ / 2 h / -20 °C

2: 1 M NaOMe / CH₂Cl₂; methanol / 2 h

3: silver silicate, molecular sieve 4 Angstroem / CH₂Cl₂ / 2.5 h / -20 °C

With silver silicate; 4 A molecular sieve; sodium methylate; In methanol; dichloromethane;

Reference yield:

: 106115-81-5
Benzyl-6-O-acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid

: 106115-83-7
Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-6-O-(4,6-di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 1 M NaOMe / CH₂Cl₂; methanol / 2 h

2: silver silicate, molecular sieve 4 Angstroem / CH₂Cl₂ / 2.5 h / -20 °C

With silver silicate; 4 A molecular sieve; sodium methylate; In methanol; dichloromethane;