zirconocene(P(2,6-Mes₂C₆H₃))P(CH₃)3

Base Information

Chemical Name:zirconocene(P(2,6-Mes₂C₆H₃))P(CH₃)3
CAS No.:252557-68-9
Molecular Formula:C₃₇H₄₄P₂Zr
Molecular Weight:641.928
Hs Code.:

zirconocene(P(2,6-Mes<sub>2</sub>C<sub>6</sub>H<sub>3</sub>))P(CH<sub>3</sub>)3

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Chemical Property of zirconocene(P(2,6-Mes₂C₆H₃))P(CH₃)3

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Technology Process of zirconocene(P(2,6-Mes₂C₆H₃))P(CH₃)3

There total 2 articles about zirconocene(P(2,6-Mes₂C₆H₃))P(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: zirconocene methyl chloride

: 478622-13-8,260998-02-5
lithium 2,6-dimesitylphenylphosphide-diethyl ether

: 594-09-2
trimethylphosphane

: 252557-68-9
zirconocene(P(2,6-Mes₂C₆H₃))P(CH₃)3

Guidance literature:: In toluene; byproducts: LiCl, CH4; (N2); addn. of lithium compd. and zirconium complex to a soln. of phosphine in toluene at room temp., keeping for 2 d; filtration, concn., filtration, washing with hexanes, drying in vac., crystn. (hot toluene/hexane 1:1); elem. anal.;
DOI:10.1016/S0022-328X(01)00863-4