2,2,4,4-tetramethyl-2,1-benzazaborinane

Base Information

Chemical Name:2,2,4,4-tetramethyl-2,1-benzazaborinane
CAS No.:1350465-74-5
Molecular Formula:C₁₂H₂₀BN
Molecular Weight:189.108
Hs Code.:

Synonyms:

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Chemical Property of 2,2,4,4-tetramethyl-2,1-benzazaborinane

Chemical Property:

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Technology Process of 2,2,4,4-tetramethyl-2,1-benzazaborinane

There total 4 articles about 2,2,4,4-tetramethyl-2,1-benzazaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350465-72-3
C₆H₅C(CH₃)2CH₂N(CH₃)2BH₃

: 1350465-76-7
1,1,4-trimethyl-4-phenyl-1,2-azaborolidine

: 1350465-74-5
2,2,4,4-tetramethyl-2,1-benzazaborinane

Guidance literature:: C₆H₅C(CH₃)2CH₂N(CH₃)2BH₃; With bis(trifluoromethanesulfonyl)amide; In toluene; at 160 ℃; for 14h; Sealed tube;

With tetrabutylammonium borohydride; In toluene;
DOI:10.1021/ja208093c

Reference yield:

: 121800-25-7
2-methyl-2-phenyl-propionic acid , dimethylamide

: 1350465-76-7
1,1,4-trimethyl-4-phenyl-1,2-azaborolidine

: 1350465-74-5
2,2,4,4-tetramethyl-2,1-benzazaborinane

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

2: bis(trifluoromethanesulfonyl)amide / toluene / 14 h / 160 °C / Sealed tube

With dimethylsulfide borane complex; bis(trifluoromethanesulfonyl)amide; In tetrahydrofuran; toluene;
DOI:10.1021/ja208093c

Reference yield:

: 826-55-1
2-methyl-2-phenylpropionic acid

: 1350465-76-7
1,1,4-trimethyl-4-phenyl-1,2-azaborolidine

: 1350465-74-5
2,2,4,4-tetramethyl-2,1-benzazaborinane

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 5 h / Reflux

2: water / 1 h / 20 °C

3: dimethylsulfide borane complex / tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

4: bis(trifluoromethanesulfonyl)amide / toluene / 14 h / 160 °C / Sealed tube

With thionyl chloride; dimethylsulfide borane complex; bis(trifluoromethanesulfonyl)amide; In tetrahydrofuran; water; toluene;
DOI:10.1021/ja208093c