(η5-C5H5)Re(NO)(PPh3)NMe2

Base Information

Chemical Name:(η5-C5H5)Re(NO)(PPh3)NMe2
CAS No.:139236-39-8
Molecular Formula:C₂₅H₂₆N₂OPRe
Molecular Weight:587.675
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η5-C5H5)Re(NO)(PPh3)NMe2

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Technology Process of (η5-C5H5)Re(NO)(PPh3)NMe2

There total 1 articles about (η5-C5H5)Re(NO)(PPh3)NMe2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126136-39-8
{(η5-C5H5)Re(NO)(PPh3)NHMe2}OTf

: 139236-39-8
(η5-C5H5)Re(NO)(PPh3)NMe2

Guidance literature:: With n-butyl lithium; In tetrahydrofuran; cyclohexane; cooling of Re-compd. in THF (-80°C), addn. of BuLi in hexane with stirring, (15 min); drying (vac., 1 h), cooling (-80°C), extn. ((D8)THF; not isolated; (1)H-, (13)C- and (31)P-NMR spectroscopy;

Reference yield:

: 139236-39-8
(η5-C5H5)Re(NO)(PPh3)NMe2

: 431-47-0
trifluoroacetic acid-methyl ester

: 126136-39-8
{(η5-C5H5)Re(NO)(PPh3)NHMe2}OTf

Guidance literature:: With triethyl amine; In tetrahydrofuran; addn. of CH3OTF to mixt. of Re-compd. and Et3N in THF (-80°C); not isolated; (1)H-NMR spectroscopy;