Technology Process of C21H26N10O7S2
There total 6 articles about C21H26N10O7S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); triphenylphosphine;
In
tetrahydrofuran;
at 30 ℃;
for 4h;
DOI:10.1016/j.bmcl.2012.06.040
- Guidance literature:
-
Multi-step reaction with 5 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.25 h / 20 °C
2: tetrabutylammomium bromide / dichloromethane; water / 30 °C
3: toluene-4-sulfonic acid / acetone / 30 h / 0 °C
4: tetrahydrofuran / 6 h / 30 °C
5: tetrakis(triphenylphosphine) palladium(0); triphenylphosphine / tetrahydrofuran / 4 h / 30 °C
With
tetrakis(triphenylphosphine) palladium(0); di-isopropyl azodicarboxylate; tetrabutylammomium bromide; toluene-4-sulfonic acid; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water; acetone;
1: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2012.06.040
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / acetone / 30 h / 0 °C
2: tetrahydrofuran / 6 h / 30 °C
3: tetrakis(triphenylphosphine) palladium(0); triphenylphosphine / tetrahydrofuran / 4 h / 30 °C
With
tetrakis(triphenylphosphine) palladium(0); toluene-4-sulfonic acid; triphenylphosphine;
In
tetrahydrofuran; acetone;
DOI:10.1016/j.bmcl.2012.06.040
