6-(4-chlorophenyl)-5H-dibenzo<1,3>diazepine

Base Information

• Chemical Name: 6-(4-chlorophenyl)-5H-dibenzo<1,3>diazepine
• CAS No.: 4509-48-2
• Molecular Formula: C₁₉H₁₃ClN₂
• Molecular Weight: 304.779

Synonyms:

Chemical Property of 6-(4-chlorophenyl)-5H-dibenzo<1,3>diazepine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 6-(4-chlorophenyl)-5H-dibenzo<1,3>diazepine

There total 3 articles about 6-(4-chlorophenyl)-5H-dibenzo<1,3>diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,1'-biphenyl-2,2'-diamine (1454-80-4) + methyl-4-chlorobenzenecarbimidothioate hydroiodide (62925-87-5) → 6-(4-chlorophenyl)-5H-dibenzo<1,3>diazepine (4509-48-2)

Guidance literature:

In ethanol; for 1h; Heating;

DOI:10.1080/00397919708004101

Reference yield:

4-chlorothiobenzamide (2521-24-6) → 6-(4-chlorophenyl)-5H-dibenzo<1,3>diazepine (4509-48-2)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone / 4 h / 60 °C

2: 93 percent / ethanol / 1 h / Heating

In ethanol; acetone;

DOI:10.1080/00397919708004101

Reference yield:

→ 6-(4-chlorophenyl)-5H-dibenzo<1,3>diazepine (4509-48-2)

Guidance literature:

4-Chlor-phenyl-formimidsaeure-ethylester-hydrochlorid, 2,2'-Diamino-biphenyl, 8-10-fache Mengen Me. bezogen auf letzteres < 65grad, 10 Min. -> 20grad, 12-16 h>; isol. als Hydrochlorid. Base aus Hydrochlorid: wss. NaOH, Ae.;

upstream raw materials:

1,1'-biphenyl-2,2'-diamine

methyl-4-chlorobenzenecarbimidothioate hydroiodide

4-chlorothiobenzamide

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