(2-ethylthiobenzoyl)ferrocene

Base Information

• Chemical Name: (2-ethylthiobenzoyl)ferrocene
• CAS No.: 1242951-48-9
• Molecular Formula: C₁₉H₁₈FeOS
• Molecular Weight: 350.264
• Mol file: 1242951-48-9.mol

Synonyms:

Chemical Property of (2-ethylthiobenzoyl)ferrocene

Chemical Property:

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Technology Process of (2-ethylthiobenzoyl)ferrocene

There total 1 articles about (2-ethylthiobenzoyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

ferrocene (102-54-5,55404-68-7) + 2-ethylsulfanylbenzoic acid (21101-79-1) → (2-ethylthiobenzoyl)ferrocene (1242951-48-9)

Guidance literature:

With PCl₃; AlCl₃; In dichloromethane; stirring overnight a mixt. of acid, ferrocene, PCl3 at room temp., addn.of AlCl3, stirring for 4 h; pouring into cold KOH soln., sepn., extn. aq. layer with CH2Cl2, washingorg. layer with water, brine, water, drying over Na2SO4, evapn., column chromy. (SiO2, light petroleum, then toluene or toluene/ethyl acetate 9 :1);

DOI:10.1016/j.poly.2010.04.034

upstream raw materials:

ferrocene

2-ethylsulfanylbenzoic acid

Refernces