2,5-Dibromo-3,6-dimethyl-4-nitroaniline

Base Information

Chemical Name:2,5-Dibromo-3,6-dimethyl-4-nitroaniline
CAS No.:120455-54-1
Molecular Formula:C8H8Br2N2O2
Molecular Weight:323.972
Hs Code.:
DSSTox Substance ID:DTXSID60558855
Wikidata:Q82441309
Mol file:120455-54-1.mol

Synonyms:2,5-Dibromo-3,6-dimethyl-4-nitroaniline;120455-54-1;DTXSID60558855

Suppliers and Price of 2,5-Dibromo-3,6-dimethyl-4-nitroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-Dibromo-3,6-dimethyl-4-nitroaniline

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:323.89320
Heavy Atom Count:14
Complexity:234

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C(=C1Br)[N+](=O)[O-])C)Br)N

Technology Process of 2,5-Dibromo-3,6-dimethyl-4-nitroaniline

There total 3 articles about 2,5-Dibromo-3,6-dimethyl-4-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.9%

: 120455-48-3
1-azido-2,5-dibromo-3,6-dimethyl-4-nitrobenzene

: 120455-54-1
2,5-dibromo-3,6-dimethyl-4-nitroaniline

Guidance literature:: With mercaptoacetic acid; triethylamine; In ethanol; at 50 - 55 ℃; for 1h;

Reference yield:

: 120455-44-9
1,4-dibromo-2,5-dimethyl-3,6-dinitro-benzene

: 120455-54-1
2,5-dibromo-3,6-dimethyl-4-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 42.5 percent / NaN₃ / dimethylsulfoxide / 0.5 h / 90 °C

2: 60.9 percent / thioglycolic acid, Et₃N / ethanol / 1 h / 50 - 55 °C

With sodium azide; mercaptoacetic acid; triethylamine; In ethanol; dimethyl sulfoxide;