Technology Process of C28H17ClN4O4
There total 3 articles about C28H17ClN4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H19ClN4O3; N,N-dimethyl-formamide;
With
silica gel; trichlorophosphate;
for 0.0583333h;
Microwave irradiation;
With
water;
In
neat (no solvent);
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrazine hydrate / ethanol / Reflux
2.1: N,N-dimethyl-formamide / 0.02 h / Microwave irradiation
3.1: trichlorophosphate; silica gel / 0.06 h / Microwave irradiation
3.2: 255
With
silica gel; hydrazine hydrate; trichlorophosphate;
In
ethanol; N,N-dimethyl-formamide;
3.2: |Vilsmeier-Haack Formylation;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N,N-dimethyl-formamide / 0.02 h / Microwave irradiation
2.1: trichlorophosphate; silica gel / 0.06 h / Microwave irradiation
2.2: 255
With
silica gel; trichlorophosphate;
In
N,N-dimethyl-formamide;
2.2: |Vilsmeier-Haack Formylation;