C₂₉H₃₅N₅O₆

Base Information

Chemical Name:C₂₉H₃₅N₅O₆
CAS No.:1581709-48-9
Molecular Formula:C₂₉H₃₅N₅O₆
Molecular Weight:549.627
Hs Code.:

C<sub>29</sub>H<sub>35</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₂₉H₃₅N₅O₆

Chemical Property:

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Technology Process of C₂₉H₃₅N₅O₆

There total 15 articles about C₂₉H₃₅N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383717-80-3
2,4-bis-(benzyloxy)-5-isopropylaniline

: 1581709-48-9
C₂₉H₃₅N₅O₆

Guidance literature:: Multi-step reaction with 8 steps

1: tert.-butylnitrite; trimethylsilylazide / acetonitrile / 13 h / 0 - 20 °C

2: chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer / N,N-dimethyl-formamide / 12 h / 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

4: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C

5: triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C

6: methanol / 80 °C / Sealed tube

7: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / 20 °C / 760.05 Torr / Sealed tube

8: perchlorate / 12 h / 20 °C

With tert.-butylnitrite; chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; trimethylsilylazide; 10 wt% Pd(OH)2 on carbon; tetrabutyl ammonium fluoride; hydrogen; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2: |Huisgen Cycloaddition;
DOI:10.1021/jm401536b

Reference yield:

: C₂₃H₂₁N₃O₂

: 1581709-48-9
C₂₉H₃₅N₅O₆

Guidance literature:: Multi-step reaction with 7 steps

1: chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer / N,N-dimethyl-formamide / 12 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

3: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C

4: triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C

5: methanol / 80 °C / Sealed tube

6: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / 20 °C / 760.05 Torr / Sealed tube

7: perchlorate / 12 h / 20 °C

With chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; 10 wt% Pd(OH)2 on carbon; tetrabutyl ammonium fluoride; hydrogen; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; 1: |Huisgen Cycloaddition;
DOI:10.1021/jm401536b

Reference yield:

: 1093190-17-0
tert-butyl[(4-ethynylphenyl)methoxy]dimethylsilane

: 1581709-48-9
C₂₉H₃₅N₅O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 1 h / -78 - -40 °C

1.2: -40 - 20 °C

2.1: chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer / N,N-dimethyl-formamide / 12 h / 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

4.1: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C

5.1: triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C

6.1: methanol / 80 °C / Sealed tube

7.1: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / 20 °C / 760.05 Torr / Sealed tube

8.1: perchlorate / 12 h / 20 °C

With chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; 10 wt% Pd(OH)2 on carbon; tetrabutyl ammonium fluoride; hydrogen; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 2.1: |Huisgen Cycloaddition;
DOI:10.1021/jm401536b