N--N-<3-(2-triphenylmethyltetrazol-5-yl)propyl>glycine ethyl ester

Base Information

Chemical Name:N--N-<3-(2-triphenylmethyltetrazol-5-yl)propyl>glycine ethyl ester
CAS No.:221106-47-4
Molecular Formula:C₄₃H₄₄N₆O₄
Molecular Weight:708.86
Hs Code.:

N-<N-(2-naphthoyl)-L-valyl>-N-<3-(2-triphenylmethyltetrazol-5-yl)propyl>glycine ethyl ester

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Chemical Property of N--N-<3-(2-triphenylmethyltetrazol-5-yl)propyl>glycine ethyl ester

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Technology Process of N--N-<3-(2-triphenylmethyltetrazol-5-yl)propyl>glycine ethyl ester

There total 4 articles about N--N-<3-(2-triphenylmethyltetrazol-5-yl)propyl>glycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 221106-47-4
N--N-<3-(2-triphenylmethyltetrazol-5-yl)propyl>glycine ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / 1-hydroxybenzotriazole, N-methylmorpholine, 1-ethyl-3-dimethylaminopropylcarbodiimide monohydrochloride / dimethylformamide / 4 h / Ambient temperature

2: trifluoroacetic acid / CH₂Cl₂ / 2 h / Ambient temperature

3: triethylamine / CHCl₃ / 1 h / 4 °C

4: 46 percent / sodium azide, ammonium chloride / dimethylformamide / 24 h / 100 °C

5: triethylamine / CHCl₃ / 2 h / Ambient temperature

With 4-methyl-morpholine; sodium azide; ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.11

Reference yield:

: [((S)-2-Amino-3-methyl-butyryl)-(3-cyano-propyl)-amino]-acetic acid ethyl ester

: 221106-47-4
N--N-<3-(2-triphenylmethyltetrazol-5-yl)propyl>glycine ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / CHCl₃ / 1 h / 4 °C

2: 46 percent / sodium azide, ammonium chloride / dimethylformamide / 24 h / 100 °C

3: triethylamine / CHCl₃ / 2 h / Ambient temperature

With sodium azide; ammonium chloride; triethylamine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.11

Reference yield:

: 221106-41-8
N-(N-tert-butoxycarbonyl-L-valyl)-N-(3-cyanopropyl)glycine ethyl ester

: 221106-47-4
N--N-<3-(2-triphenylmethyltetrazol-5-yl)propyl>glycine ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / CH₂Cl₂ / 2 h / Ambient temperature

2: triethylamine / CHCl₃ / 1 h / 4 °C

3: 46 percent / sodium azide, ammonium chloride / dimethylformamide / 24 h / 100 °C

4: triethylamine / CHCl₃ / 2 h / Ambient temperature

With sodium azide; ammonium chloride; triethylamine; trifluoroacetic acid; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.11