9a-tert-butyl-2-phenyl-3,4-cyclohexeno-4a,9-diaza-1,2,4a,9a-tetrahydrofluorene

Base Information

Chemical Name:9a-tert-butyl-2-phenyl-3,4-cyclohexeno-4a,9-diaza-1,2,4a,9a-tetrahydrofluorene
CAS No.:78530-97-9
Molecular Formula:C₂₅H₃₀N₂
Molecular Weight:358.527
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9a-tert-butyl-2-phenyl-3,4-cyclohexeno-4a,9-diaza-1,2,4a,9a-tetrahydrofluorene

Chemical Property:

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Technology Process of 9a-tert-butyl-2-phenyl-3,4-cyclohexeno-4a,9-diaza-1,2,4a,9a-tetrahydrofluorene

There total 4 articles about 9a-tert-butyl-2-phenyl-3,4-cyclohexeno-4a,9-diaza-1,2,4a,9a-tetrahydrofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 78530-95-7
4,4-dimethyl-1-phenyl-1-(2'-oxocyclohexyl)-3-pentanone

: 95-54-5
1,2-diamino-benzene

: 78530-97-9
9a-tert-butyl-2-phenyl-3,4-cyclohexeno-4a,9-diaza-1,2,4a,9a-tetrahydrofluorene

Guidance literature:

Reference yield:

: 538-44-3
4,4-dimethyl-1-phenyl-1-penten-3-one

: 78530-97-9
9a-tert-butyl-2-phenyl-3,4-cyclohexeno-4a,9-diaza-1,2,4a,9a-tetrahydrofluorene

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / sodium hydroxide

With sodium hydroxide;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 78530-97-9
9a-tert-butyl-2-phenyl-3,4-cyclohexeno-4a,9-diaza-1,2,4a,9a-tetrahydrofluorene

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 40percent aq. NaOH / ethanol / 24 h / Ambient temperature

2: 48 percent / p-toluenesulfonic acid / xylene / Heating

With sodium hydroxide; toluene-4-sulfonic acid; In ethanol; xylene;
DOI:10.1007/BF00842840