disparlure

Base Information

• Chemical Name: disparlure
• CAS No.: 54910-54-2
• Molecular Formula: C₁₉H₃₈O
• Molecular Weight: 282.51
• Mol file: 54910-54-2.mol

Synonyms:

Chemical Property of disparlure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of disparlure

There total 40 articles about disparlure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

cis-2-Methyl-7-octadecen (35354-39-3) → disparlure (29804-22-6,35898-62-5,42991-03-7,54910-51-9,54910-52-0,54910-53-1,54910-54-2,57457-72-4,65634-82-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid;

DOI:10.1055/s-1983-30302

Reference yield:

trans-7,8-epoxy-2-methyloctadecane (51050-50-1) → disparlure (29804-22-6,35898-62-5,42991-03-7,54910-51-9,54910-52-0,54910-53-1,54910-54-2,57457-72-4,65634-82-4) + trans-7,8-epoxy-2-methyloctadecane (42991-03-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; Title compound not separated from byproducts;

DOI:10.1016/0022-328X(85)87361-7

Reference yield:

2-methyloctadec-7-yne (35354-38-2) → disparlure (29804-22-6,35898-62-5,42991-03-7,54910-51-9,54910-52-0,54910-53-1,54910-54-2,57457-72-4,65634-82-4)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Lindlar / ethanol / Ambient temperature

2: m-chloroperoxybenzoic acid / CH₂Cl₂ / 0 °C

With hydrogen; 3-chloro-benzenecarboperoxoic acid; Lindlar's catalyst; In ethanol; dichloromethane;

upstream raw materials:

cis-2-Methyl-7-octadecen

4-methylpentyllithium

(3-decyloxiran-2-yl)methyl 4-methylbenzenesulfonate

trans-7,8-epoxy-2-methyloctadecane