C₂₂H₂₈N₄O

Base Information

Chemical Name:C₂₂H₂₈N₄O
CAS No.:1365534-23-1
Molecular Formula:C₂₂H₂₈N₄O
Molecular Weight:364.491
Hs Code.:

C<sub>22</sub>H<sub>28</sub>N<sub>4</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₈N₄O

Chemical Property:

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Technology Process of C₂₂H₂₈N₄O

There total 7 articles about C₂₂H₂₈N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1365534-22-0
C₂₈H₄₂N₄O₂Si

: 1365534-23-1
C₂₂H₂₈N₄O

Guidance literature:: With tetrabutyl ammonium fluoride; ethylenediamine; In N,N-dimethyl-formamide; at 85 ℃;
DOI:10.1016/j.bmcl.2012.01.041

Reference yield:

: 98027-84-0
2,6-dichloro-4-iodopyridine

: 1365534-23-1
C₂₂H₂₈N₄O

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / Reflux

2: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; ethanol; water / 170 °C / Microwave irradiation

3: potassium hydroxide / ethanol; water / 50 °C

4: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tert-butyl alcohol / 130 °C / Microwave irradiation

6: tetrabutyl ammonium fluoride; ethylenediamine / N,N-dimethyl-formamide / 85 °C

With bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; tetrabutyl ammonium fluoride; sodium hydride; sodium carbonate; ethylenediamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.01.041

Reference yield:

: 1356998-56-5
2-tert-butoxy-6-chloro-4-iodopyridine

: 1365534-23-1
C₂₂H₂₈N₄O

Guidance literature:: Multi-step reaction with 5 steps

1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; ethanol; water / 170 °C / Microwave irradiation

2: potassium hydroxide / ethanol; water / 50 °C

3: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tert-butyl alcohol / 130 °C / Microwave irradiation

5: tetrabutyl ammonium fluoride; ethylenediamine / N,N-dimethyl-formamide / 85 °C

With bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; tetrabutyl ammonium fluoride; sodium hydride; sodium carbonate; ethylenediamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium hydroxide; In 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.01.041