(S,E)-4-(1-(1-(4-((2-carboxyethyl)carbamoyl)phenyl)ethyl)-3-(3,5-dichlorophenyl)-1H-pyrazol-5-yl)-2-(3-methoxy-3-oxoprop-1-en-1-yl)benzoic acid

Base Information

• Chemical Name: (S,E)-4-(1-(1-(4-((2-carboxyethyl)carbamoyl)phenyl)ethyl)-3-(3,5-dichlorophenyl)-1H-pyrazol-5-yl)-2-(3-methoxy-3-oxoprop-1-en-1-yl)benzoic acid
• CAS No.: 1429779-45-2
• Molecular Formula: C₃₂H₂₇Cl₂N₃O₇
• Molecular Weight: 636.488

Synonyms:

Chemical Property of (S,E)-4-(1-(1-(4-((2-carboxyethyl)carbamoyl)phenyl)ethyl)-3-(3,5-dichlorophenyl)-1H-pyrazol-5-yl)-2-(3-methoxy-3-oxoprop-1-en-1-yl)benzoic acid

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Technology Process of (S,E)-4-(1-(1-(4-((2-carboxyethyl)carbamoyl)phenyl)ethyl)-3-(3,5-dichlorophenyl)-1H-pyrazol-5-yl)-2-(3-methoxy-3-oxoprop-1-en-1-yl)benzoic acid

There total 2 articles about (S,E)-4-(1-(1-(4-((2-carboxyethyl)carbamoyl)phenyl)ethyl)-3-(3,5-dichlorophenyl)-1H-pyrazol-5-yl)-2-(3-methoxy-3-oxoprop-1-en-1-yl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-3-(4-(1-(3-(3,5-dichlorophenyl)-5-(6-methoxynaphthalen-2-yl)-1Hpyrazol-1-yl)ethyl)benzamido)propanoic acid → (S)-3-(4-(1-(3-(3,5-dichlorophenyl)-5-(6-methoxy-5,8-dioxo-5,8-dihydronaphthalen-2-yl)-1H-pyrazol-1-yl)ethyl)benzamido)propanoic acid (1429779-44-1) + (S,E)-4-(1-(1-(4-((2-carboxyethyl)carbamoyl)phenyl)ethyl)-3-(3,5-dichlorophenyl)-1H-pyrazol-5-yl)-2-(3-methoxy-3-oxoprop-1-en-1-yl)benzoic acid (1429779-45-2)

Guidance literature:

With methanol; 4,4'-dicyano-4,4'-azo-di-valeric acid; In water; acetonitrile; at 40 ℃; for 72h;

DOI:10.1002/jps.23500

Reference yield:

(S)-3-(4-(1-(3-(3,5-dichlorophenyl)-5-(6-methoxynaphthalen-2-yl)-1Hpyrazol-1-yl)ethyl)benzamido)propanoic acid → (S)-3-(4-(1-(5-(5-((2-cyanopropan-2-yl)oxy)-6-methoxynaphthalen-2-yl)-3-(3,5-dichlorophenyl)-1H-pyrazol-1-yl)ethyl)benzamido)propanoic acid (1429779-43-0) + (S)-3-(4-(1-(3-(3,5-dichlorophenyl)-5-(6-methoxy-5,8-dioxo-5,8-dihydronaphthalen-2-yl)-1H-pyrazol-1-yl)ethyl)benzamido)propanoic acid (1429779-44-1) + (S,E)-4-(1-(1-(4-((2-carboxyethyl)carbamoyl)phenyl)ethyl)-3-(3,5-dichlorophenyl)-1H-pyrazol-5-yl)-2-(3-methoxy-3-oxoprop-1-en-1-yl)benzoic acid (1429779-45-2)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In water; acetonitrile; at 40 ℃; for 72h;

DOI:10.1002/jps.23500

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