propenyl Δ¹-cyclohexenyl ketone

Base Information

• Chemical Name: propenyl Δ¹-cyclohexenyl ketone
• CAS No.: 15450-53-0
• Molecular Formula: C₁₀H₁₄O
• Molecular Weight: 150.221
• Mol file: 15450-53-0.mol

Synonyms:

Chemical Property of propenyl Δ¹-cyclohexenyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of propenyl Δ¹-cyclohexenyl ketone

There total 1 articles about propenyl Δ¹-cyclohexenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ propenyl Δ1-cyclohexenyl ketone (15450-53-0)

Guidance literature:

Cyclohexen, Vinylacetylbromid (2) / AlCl3;

DOI:10.1039/C39790000263

Reference yield: 50.5%

propenyl Δ1-cyclohexenyl ketone (15450-53-0) + phenylphosphane (638-21-1) → 3-methyl-2-phenyl-2-phosphabicyclo<4.4.0>decan-5-one (53097-93-1)

Guidance literature:

at 140 - 150 ℃; for 2h;

Reference yield: 4.0%

propenyl Δ1-cyclohexenyl ketone (15450-53-0) + 2-phenyl-2-thioxo-2-phosphabicyclo<4.4.0>decan-5-one (87669-37-2,118918-17-5,119944-94-4,119944-95-5,119944-98-8,120020-19-1,128525-80-4) → 2-Phenyl-4-(1-methyl-3-cyclohexen-1-yl-3-oxopropyl)-2-thioxo-2-phosphabicyclo<4.4.0>decan-5-one (134284-08-5) + 2-Methyl-13-phenyl-13-thioxo-13-phosphatetracyclo<9.7.01,14.05,10.11,10>nonadecane-4,19-dione (134284-10-9)

Guidance literature:

With sodium hydroxide; In ethanol; for 2.5h; Heating;

Downstream raw materials:

1-cyclohex-1-enyl-3-dimethylamino-butan-1-one

1-cyclohex-1-enyl-but-2c-en-1-one-(2,4-dinitro-phenylhydrazone)

1-cyclohex-1-enyl-but-2t-en-1-one-(2,4-dinitro-phenylhydrazone)

3-methyl-2-phenyl-2-phosphabicyclo<4.4.0>decan-5-one