Technology Process of C29H29N5O5
There total 11 articles about C29H29N5O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water
2: dicyclohexyl-carbodiimide; dmap; benzotriazol-1-ol / N,N-dimethyl-formamide
3: trifluoroacetic acid; methoxybenzene
4: sodium hydroxide; water / water; 1,4-dioxane
With
dmap; sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; water; benzotriazol-1-ol; methoxybenzene; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium hydroxide;
In
1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.06.028
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N,N',N'-trimethylenediamine; n-butyllithium / tetrahydrofuran; hexane; cyclohexane
2: bis-triphenylphosphine-palladium(II) chloride; copper(II) oxide / N,N-dimethyl-formamide / 110 °C
3: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water
4: dicyclohexyl-carbodiimide; dmap; benzotriazol-1-ol / N,N-dimethyl-formamide
5: trifluoroacetic acid; methoxybenzene
6: sodium hydroxide; water / water; 1,4-dioxane
With
dmap; bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; n-butyllithium; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; water; benzotriazol-1-ol; N,N',N'-trimethylenediamine; methoxybenzene; dicyclohexyl-carbodiimide; trifluoroacetic acid; copper(II) oxide; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; hexane; cyclohexane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.06.028
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bis-triphenylphosphine-palladium(II) chloride; copper(II) oxide / N,N-dimethyl-formamide / 110 °C
2: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water
3: dicyclohexyl-carbodiimide; dmap; benzotriazol-1-ol / N,N-dimethyl-formamide
4: trifluoroacetic acid; methoxybenzene
5: sodium hydroxide; water / water; 1,4-dioxane
With
dmap; bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; water; benzotriazol-1-ol; methoxybenzene; dicyclohexyl-carbodiimide; trifluoroacetic acid; copper(II) oxide; sodium hydroxide;
In
1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.06.028